Relay liquid state epoxy resin pouring sealant and preparation method thereof
A technology of liquid epoxy resin and epoxy resin, which is applied in the direction of epoxy resin glue, chemical instruments and methods, adhesives, etc., can solve the problems of deterioration of packaging product characteristics, high curing temperature, poor temperature resistance of relay plastic shells, etc., to achieve Wide range of effects
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[0085] Experimental example 1
[0086] In grams, weigh 20.5 parts of high-purity bisphenol A epoxy resin (828EL), 35.3 parts of electronic grade bisphenol F diglycidyl ether (830s), 0.5 parts of black paste, and 4.6 parts of dicyandiamide curing agent. 1.5 parts of curing accelerator, 2.0 parts of coupling agent (KH560), 92 parts of alumina spherical filler were prepared according to the above preparation method to obtain sample 1.
[0087] After testing, the curing temperature is 110℃ for 20 minutes, the shear strength is 13MPa, the coefficient of linear expansion (CTE) a1 is 20ppm, the Tg point is 137℃, the thermal conductivity is 1.0w / mk, and the storage period is more than 10h at 40℃. The storage period at 8°C is 10 months.
Example Embodiment
[0088] Experimental example 2
[0089] In grams, weigh 20 parts of high-purity bisphenol A epoxy resin (828EL), 40.0 parts of electronic grade bisphenol F diglycidyl ether (830s), 0.5 parts of black paste, and 5.4 parts of dicyandiamide curing agent. 0.5 parts of curing accelerator, 2.0 parts of coupling agent KH560, and 80 parts of alumina spherical filler were prepared according to the above preparation method to obtain sample 2.
[0090] After testing, the curing temperature of sample 2 is 110℃ for 20 minutes, and the shear strength is 10MPa; the storage period at 40℃ exceeds 10h, and the storage period at 2-8℃ is 10 months.
Example Embodiment
[0091] Experimental example 3
[0092] In grams, weigh 25 parts of high-purity bisphenol A epoxy resin (828EL), 35.0 parts of electronic grade bisphenol F diglycidyl ether (830s), 0.5 parts of black paste, and dicyandiamide curing agent: 5.4 parts , 0.5 parts of curing accelerator, 1.5 parts of KH560 coupling agent, 80 parts of alumina spherical filler, prepared according to the above preparation method, to obtain sample 3.
[0093] After testing, the curing temperature of sample 3 is 110°C for 20 minutes, and the shear strength is 11MPa; the storage period at 40°C exceeds 10 hours, and the storage period at 2-8°C is 10 months.
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