External compound scorpion composition for treating age spots, chloasma, skin pigmentation and solar dermatitis, its preparation method and application
A technology for skin pigmentation and chloasma, which is used in medical preparations containing active ingredients, drug combinations, skin diseases, etc., and can solve problems such as easy recurrence, immune dysfunction of skin defense tissue, and residual pigmentation.
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experiment example 1
[0014] Experimental example 1: Chemical research on the high temperature treatment of scorpion and centipede
[0015] Scorpion and centipede 1.72 kg of high-temperature treatment products with a weight ratio of 10:3 were extracted with 95% ethanol at 8 times the volume, heated and refluxed for 3 times, each time for 2 hours, filtered, and recovered under reduced pressure to obtain ethanol Extract 216g. Take 216g of the ethanol extract and carry out rough separation by silica gel column chromatography, and elute with petroleum ether-ethyl acetate solvent system. It was separated by modern separation techniques and methods such as gel column chromatography, and a total of 6 monomeric compounds were obtained. Through chemical analysis and comprehensive analysis of various spectral data, the chemical structures of six monomer compounds were determined, and the data were assigned. The separation process is shown in the table below.
[0016]
[0017] Compound 1 is a colorless n...
experiment example 2
[0024] Experimental example 2: GC-MS chemical composition analysis of scorpions, centipedes and their mixed medicinal materials after high temperature treatment
[0025] Scorpion, centipede and their mixed medicinal materials with a weight ratio of 10:5 are subjected to high temperature treatment according to the following method: take vaseline with a mass ratio of 1:1 to the medicinal material, heat and melt at 60-70°C, and mix scorpion, centipede and Mix medicinal materials, add molten vaseline and mix evenly, place in the heating room, gradually increase the temperature, the maximum temperature is 220°C, and keep the temperature at 190°C for no less than 30 minutes, and keep the time at 200-210°C for no less than 40 minutes , that is, high-temperature processed products of scorpion, centipede and mixed medicinal materials.
[0026] Accurately weigh 5g of the above-mentioned high-temperature treatment product, add 100mL of 95% ethanol, and extract under reflux for 3h, then c...
Embodiment 1
[0035] Embodiment 1: Combine the mixed extract of scorpion and centipede high temperature treatment with borneol and vaseline to make external ointment
[0036] (1) Make oil-in-water emulsion for external use
[0037] Take the original medicinal materials of scorpion, centipede and borneol with a weight ratio of 5:1:2, and prepare according to the following steps:
[0038] (1) High-temperature treatment of scorpions and centipedes: take the original medicinal materials of scorpions and centipedes, add vaseline with 3 times the weight of the composition of the two, heat and melt at 70°C, add the medicinal materials of scorpions and centipedes into molten vaseline and mix evenly , put it in an oven, gradually increase the temperature, the highest temperature is 220°C, among which the constant temperature is kept at 190°C for no less than 30 minutes, and the time at 200-210°C is not less than 40 minutes, take it out, let it cool, and you can get the scorpion, High-temperature tr...
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