Ceramic composite material and method for processing members
A technology for ceramic composite materials and components, applied in the field of materials, can solve the problems of high alumina sintering temperature and high dielectric constant, and achieve the effect of reducing sintering temperature and reducing dielectric loss
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Embodiment 1
[0022] Weigh SiO according to the chemical composition in the table below 2 , H 3 BO 3 , (NH 4 )H 2 PO 4 , ZnO
[0023]
SiO 2
B 2 o 3
P 2 o 5
ZnO
wt%
75
15
6
4
[0024] Add the weighed raw materials into ethanol, use alumina as a ball mill in a planetary ball mill for 4 hours, then dry at 80°C for 6 hours, and then pre-fire the dried glass powder at 400°C;
[0025] Mix the calcined 5wt% glass powder and 95wt% alumina powder, add ethanol and binder for ball milling, dry and pass through a 60-mesh sieve to granulate, and then press to form under a pressure of 120MPa. The final product is heated slowly to 500°C at a rate of 1°C / min, and held for 1 hour to ensure that the binder is completely removed, and then heated to the highest sintering temperature of 1300°C at 10°C / min, kept for 3 hours, and then Cool down to 400°C at a rate of 20°C / min, and finally cool down to room temperature with the furnace ...
Embodiment 2
[0028] Weigh SiO according to the chemical composition in the table below 2 , H 3 BO 3 , (NH 4 )H 2 PO 4 , ZnO
[0029]
SiO 2
B 2 o 3
P 2 o 5
ZnO
wt%
75
15
6
4
[0030] Add the weighed raw materials into ethanol, use alumina as a ball mill in a planetary ball mill for 4 hours, then dry at 80°C for 6 hours, and then pre-fire the dried glass powder at 400°C;
[0031] Mix the calcined 15wt% glass powder and 85wt% alumina powder, add ethanol and binder for ball milling, dry and pass through a 60-mesh sieve to granulate, and then press to form under a pressure of 120MPa. The final product is heated slowly to 500°C at a rate of 1°C / min, and held for 1 hour to ensure that the binder is completely removed, and then heated to the highest sintering temperature of 1200°C at 10°C / min, kept for 3 hours, and then Cool down to 400°C at a rate of 20°C / min, and finally cool down to room temperature with the furnace...
Embodiment 3
[0034] Weigh SiO according to the chemical composition in the table below 2 , H 3 BO 3 , (NH 4 )H 2 PO 4 , ZnO
[0035]
SiO 2
B 2 o 3
P 2 o 5
ZnO
wt%
75
15
6
4
[0036] Add the weighed raw materials into ethanol, use alumina as a ball mill in a planetary ball mill for 4 hours, then dry at 80°C for 6 hours, and then pre-fire the dried glass powder at 400°C;
[0037] Mix the calcined 30wt% glass powder and 70wt% alumina powder, add ethanol and binder for ball milling, dry and pass through a 60-mesh sieve to granulate, and then press to form under a pressure of 120MPa. The final product is heated slowly to 500°C at a rate of 1°C / min, and held for 1 hour to ensure that the binder is completely removed, and then heated to the highest sintering temperature of 1100°C at 10°C / min, kept for 3 hours, and then Cool down to 400°C at a rate of 20°C / min, and finally cool down to room temperature with the furnace...
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