A kind of interface heat conduction sheet and its preparation method, heat dissipation system
A heat conduction sheet and interface technology, applied in the field of interface heat conduction sheet and its preparation, and heat dissipation system, can solve the problem that the interface heat conduction material cannot meet the thermal conductivity at the same time, and achieve easy industrial production and use, reduce contact thermal resistance, and convenient installation Effect
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[0050] In a second aspect, an embodiment of the present invention provides a method for preparing an interface heat conduction sheet, including the following steps:
[0051] The substrate is fixed in the reaction chamber by a clamp, the reaction chamber is heated to 700-1200°C under a protective gas atmosphere, carbon source gas is introduced, and the reaction is kept at a constant temperature for 2-20 minutes; the substrate is a flexible composite Metal film or flexible graphite, the base material has a first surface and a second surface relative to the first surface, the first surface and the second surface of the base material are loaded with a catalyst, and the flexible composite metal film is surface-coated Flexible metal films coated with nickel, silver or gold;
[0052] After the reaction is completed, cool to room temperature under a protective gas atmosphere to obtain a base material with carbon nanomaterials grown on both the first surface and the second surface, tha...
Embodiment 1
[0085] A method for preparing an interface heat conduction sheet, comprising the steps of:
[0086] (1) Pretreatment of flexible composite metal film: Plating metal nickel on the surface of electrolytic copper foil according to the conventional electroplating method (it can be required that the copper foil manufacturer has prepared the corresponding inert coating treatment) to obtain a nickel-plated electrolytic coating with a thickness of 12um. The copper foil is a flexible composite metal film, which is cleaned by deionization and acetone ultrasonically, and then treated with argon plasma for 1 min after drying; nickel nitrate and deionized water are mixed to prepare a 0.02mol / L nickel nitrate solution; the flexible Soak the composite metal film in nickel nitrate solution for 30s, place the soaked flexible composite metal film in a vacuum drying oven at 90°C for 2 hours, then take it out and put it into a quartz boat, in the constant temperature zone of the quartz reaction tu...
Embodiment 2
[0090] A method for preparing an interface heat conduction sheet, comprising the steps of:
[0091] Take flexible graphite, recommended as highly oriented pyrolytic graphite (Panasonic's PGS graphite film) as the base material, the base material has a first surface and a second surface opposite to the first surface. Put Panasonic's PGS graphite film into a tube-type resistance furnace, heat it to a reaction temperature of about 850°C under the protection of argon, and then feed in hydrogen gas with a flow rate of 300 sccm and argon gas with a flow rate of 1000 sccm, and simultaneously add a concentration of 0.025 g / ml The ferrocene-dissolved xylene solution was continuously fed into the reaction chamber, and the flow rate was controlled at 0.4 mL / min. Under the transport of hydrogen and argon, the ferrocene and xylene reach the position of the PGS graphite film, and the Fe atomic clusters generated by the decomposition of ferrocene will be supported on the first surface and th...
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