Active coverage system for in-situ control of surface water bottom sediment nitrogen and phosphorus release and method
A sediment, nitrogen and phosphorus technology, applied in chemical instruments and methods, water/sludge/sewage treatment, river regulation, etc., can solve problems such as slow fixation rate, reduction effect, and unsatisfactory efficiency, and achieve bottom reduction Sludge nitrogen and phosphorus release, fast fixation rate and high fixation efficiency
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Embodiment 1
[0029] Firstly, prepare various sediment active covering materials.
[0030] 1. Synthesis of hydroxyapatite (abbreviated as HAP) by solution precipitation method. 50mL concentration of 1mol / L Ca(NO 3 ) 2 solution and 30mL concentration of 1mol / L (NH 4 ) 2 HPO 4The solution is mixed with 0.8mol / LNH 3 OH solution to adjust the pH to 9, then place the mixture in a shaker, shake at a speed of 150 rpm for 48 hours, take the precipitate and wash it to neutral, dry it to obtain apatite, and then crush it into a particle size of 200 mesh particles. Repeat the above process 4 times, and collect all the apatite samples for later use.
[0031] 2. Preparation of calcium-modified zeolite (abbreviated as CaMZ). Prepare Ca with a concentration of 1mol / L 2+ Solution; Weigh the natural zeolite with a particle size of over 80 mesh and place it in a container, then pipette Ca according to the liquid-solid ratio of 5mL / g 2+ The solution is fully mixed with the natural zeolite; after 40 ...
Embodiment 2
[0041] 1. Synthesis of hydroxyapatite (abbreviated as HAP) by solution precipitation method. 50mL concentration of 1mol / L Ca(NO 3 ) 2 solution and 30mL concentration of 1mol / L (NH 4 ) 2 HPO 4 The solution is mixed with 0.8mol / LNH 3 OH solution to adjust the pH to 9, then place the mixture in a shaker, shake at a speed of 150 rpm for 48 hours, take the precipitate and wash it to neutral, dry it to obtain apatite, and then crush it into a particle size of 200 mesh particles. Repeat the above process 4 times, and collect all the apatite samples for later use.
[0042] Preparation of calcium-modified zeolite (abbreviated as CaMZ). Prepare Ca with a concentration of 1mol / L 2+ solution (calcium nitrate or calcium chloride); weigh the natural zeolite with a particle size over 80 mesh and place it in a container, then pipette the Ca 2+ The solution is fully mixed with the natural zeolite; after 40 hours of reaction, the solid-liquid separation, cleaning and drying can be carr...
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