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Preparation method of water-soluble paprika red pigment

A technology of capsanthin and its production method, which is applied in the field of production of water-soluble capsanthin, which can solve the problem of unstable properties and properties of water-soluble capsanthin, inability to meet the requirement of diluent clarity, low utilization rate of capsanthin, etc. problem, to achieve the effect of low operating cost, fresh color, convenient storage and transportation

Inactive Publication Date: 2014-03-19
云南宏绿辣素有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The hydrolysis reaction of oil-soluble capsanthin by this technical scheme is only for the subsequent spray drying treatment, the utilization rate of capsanthin is low, the energy consumption of required equipment is large, and the production cost is high. The properties and properties of capsanthin are unstable and cannot meet the requirement of diluent clarity

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0011] Take 50 grams of oil-soluble capsanthin with a color value of 201 as a raw material, then dissolve 2.5 grams of KOH in 47.5 grams of ethanol solution (concentration is 95%) to prepare 50 grams of KOH ethanol solution, and slowly add KOH ethanol solution to the oil-soluble In the capsanthin raw material, under the condition of 55° C., the saponification reaction is carried out with stirring, and the reaction time is 4 hours.

[0012] After the saponification reaction is completed, add 15 grams of ethanol (concentration is 95%), stir evenly and cool to room temperature, carry out centrifugation at 1000r / min, take the supernatant under the condition of pressure 0.05MPa, temperature 60 ℃, concentrate and distill to recover ethanol , to obtain 58.9 grams of alcohol-soluble capsanthin with a color value of 150.1 (accounting for 87.8% of the input pigment), and centrifuging to obtain 4.5 grams of ethanol insoluble matter with a color value of 268 (accounting for 12% of the inpu...

example 2

[0016] Take 100 grams of oil-soluble capsanthin with a color value of 200 as raw material, then dissolve 10 grams of KOH in 90 grams of ethanol solution (concentration is 95%) to prepare 100 grams of KOH ethanol solution, and slowly add KOH ethanol solution to the oil-soluble In the capsanthin raw material, the saponification reaction was carried out with stirring at 60° C., and the reaction time was 5 hours.

[0017] After the saponification reaction is completed, add 30 grams of ethanol (concentration is 95%), stir evenly and cool to room temperature, carry out centrifugation at 1500r / min, take the supernatant under the condition of pressure 0.07MPa, temperature 50 ℃, concentrate and distill to recover ethanol , to obtain 101 grams of alcohol-soluble capsanthin with a color value of 171.3 (accounting for 86.5% of the input pigment), 10 grams of ethanol insoluble matter obtained by centrifugation, and a color value of 240 (accounting for 12% of the input pigment), which is res...

Embodiment 3

[0021] Take 100 grams of oil-soluble capsanthin with a color value of 190 as raw material, then dissolve 15 grams of KOH in 85 grams of ethanol solution (concentration is 95%) to prepare 100 grams of KOH ethanol solution, and slowly add KOH ethanol solution to oil-soluble capsicum In the red pigment raw material, the saponification reaction was carried out with stirring at 65° C., and the reaction time was 6 hours.

[0022] After the saponification reaction is completed, add 40 grams of ethanol (concentration is 95%), stir evenly and cool to room temperature, carry out centrifugation at 2000r / min, take the supernatant under the condition of pressure 0.08MPa, temperature 35 ℃, concentrate and distill to recover ethanol , to obtain 102 grams of alcohol-soluble capsanthin (accounting for 88% of the input pigment) with a color value of 163.9, and 10.5 grams of ethanol insoluble matter obtained by centrifugation, with a color value of 208.1 (accounting for 11.5% of the input pigment...

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Abstract

The invention discloses a preparation method of a water-soluble paprika red pigment. The preparation method comprises the following steps: adding equal amount of a solution prepared from alkali and alcohol in proportion to an oil-soluble paprika red pigment serving as a raw material, performing saponification under constant-temperature stirring condition; adding an alcohol solvent, stirring, cooling to room temperature, performing centrifugal separation, reducing pressure of a liquid supernatant, heating and distilling the liquid supernatant, recycling alcohol to obtain an alcohol-soluble paprika red pigment; adding an emulsifying agent, mixing uniformly for emulsifying; adding water according to requirement and uniformly stirring to obtain the water-soluble paprika red pigment; dissolving undissolved substances in ethyl acetate, stirring, filtering, recycling ethyl acetate by performing reduced pressure distillation on a filter liquor, and extracting residual paprika red pigment. The use rate of the pigment is over 95 percent, the prepared water-soluble paprika red pigment is stable in performance, is of bright color and is transparent after being diluted, is short in process route, low in device cost, low in operation cost and convenient to store and transport, and can be put into industrialization easily.

Description

technical field [0001] The invention relates to a preparation method of water-soluble capsanthin. Background technique [0002] Capsanthin is a carotenoid pigment present in peppers, which is usually extracted from mature red pepper fruits. It is a non-toxic and safe natural pigment that can improve human immunity, delay cell and body aging, prevent It has unique health care functions such as cancer and weight loss, and is widely used in the coloring of various foods and medicines such as aquatic products, meat, cakes, salads, canned food, beverages, etc., and can also be used in the production of cosmetics. Capsanthin without special treatment is a deep red oil-soluble liquid with bright color and strong tinting power. It is only soluble in organic solvents such as oil or ethanol, and is difficult to dissolve in water, which greatly limits the application of capsanthin. Therefore, water-soluble capsanthin has become a hot topic in the deep processing of capsanthin. [000...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09B67/54
Inventor 韦勇刘玉申黄涛马春艳罗永梅
Owner 云南宏绿辣素有限公司
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