Fluorescence reaction detector and sulfur dioxide automatic monitoring device using same

A fluorescence reaction and detector technology, which is applied in fluorescence/phosphorescence, material excitation analysis, etc., can solve the problems of large amount of instrument maintenance, fast light intensity attenuation, complex optical path, etc., and achieve extended maintenance time, good stability and small size Effect

Inactive Publication Date: 2014-03-26
HEBEI SAILHERO ENVIRONMENTAL PROTECTION HIGH TECH
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Problems solved by technology

SO of most manufacturers 2 The working principle of the automatic monitoring instrument is the non-pulse ultraviolet fluorescence method. The ultraviolet lamp used is a zinc lamp. Its light intensity decays quickly, its life is short, the maintenance of the instrument is large, and the price is high; the principle adopted by American THERMO-FISHER is ultraviolet pulse fluorescence. In this method, the ultraviolet lamp adopts a pulsed xenon lamp, and its light source has a long service life, but the optical path part needs to use 4 reflectors, the optical path is complicated, and the cost is high

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  • Fluorescence reaction detector and sulfur dioxide automatic monitoring device using same
  • Fluorescence reaction detector and sulfur dioxide automatic monitoring device using same
  • Fluorescence reaction detector and sulfur dioxide automatic monitoring device using same

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Embodiment Construction

[0031] like figure 1 , figure 2 As shown, the detector for detecting weak fluorescent signals of the present invention includes a pulsed xenon lamp light source 1 installed at one end of the tubular reaction chamber 6, and the pulsed xenon lamp light source 1 and the tubular reaction chamber 6 are sequentially installed with the reaction chamber 6. A biconvex lens 9, an optical filter 10, a plano-convex lens 11 and an aperture 12 are provided with a photomultiplier tube 3 at the top of the tubular reaction chamber 6 on one side of the corresponding aperture 12, and the photomultiplier tube 3 is a photomultiplier tube for digital signal output, It has a high signal-to-noise ratio, does not require refrigeration, and is not easily affected by ambient temperature. A lenticular lens 13 and an optical filter 15 are sequentially arranged between the photomultiplier tube 3 and the reaction chamber 6 , and the inner wall of the reaction chamber 6 is coated with an anti-corrosion coa...

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Abstract

The invention discloses a fluorescence reaction detector and a sulfur dioxide automatic monitoring device using the fluorescence reaction detector. The fluorescence reaction detector comprises a xenon lamp light source arranged at one end of a reaction chamber, wherein a biconvex lens, an optical filter, a planoconvex lens and a diaphragm are sequentially arranged between the xenon lamp light source and the reaction chamber, a photomultiplier is arranged on the reaction chamber, and a biconvex lens is arranged between the photomultiplier and the reaction chamber. The sulfur dioxide automatic monitoring device comprises a fluorescence detector, a hydrocarbon removing device, a particle filter, a vacuum pump, a sensor and a data acquisition transmission device, which are arranged in a case; the outlet of the particle filter passes through a three-way valve and is connected with a gas inlet of the fluorescence detector through an inner tube of the hydrocarbon removing device, a gas outlet of the fluorescence detector is connected with an inlet of the vacuum pump after passing through the sensor and an outer tube of the hydrocarbon removing device sequentially, the inlet of the particle filter is connected with a sampling port, and the sensor is electrically connected with the data acquisition transmission device. The fluorescence reaction detector and the sulfur dioxide automatic monitoring device can detect weak fluorescence signals of sulfur dioxide reaction and can accurately measure sulfur dioxide gas concentration value, and the light source has long service life and good stability.

Description

technical field [0001] The invention relates to a detector for detecting weak fluorescent signals and a monitoring device using the detector to monitor the concentration of sulfur dioxide gas in the air, belonging to the technical field of atmospheric monitoring equipment. Background technique [0002] With the rapid growth of the social economy and the continuous improvement of the level of urbanization, the characteristics of ambient air pollution have undergone significant changes. The problem of regional air pollution is becoming more and more serious. Compound air pollution problems such as haze, photochemical smog and acid rain are more prominent, affecting human health. And ecological security, and even the harmonious development of social economy. [0003] SO 2 It is the main pollutant component in the ambient air and an important monitoring item for environmental monitoring stations at all levels to evaluate the urban air environment quality. Among the six standar...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/64
Inventor 王强段兆丽郑雷玉王春迎张艳伟辛继国
Owner HEBEI SAILHERO ENVIRONMENTAL PROTECTION HIGH TECH
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