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Process and device for two-step sugar production

A two-step method and process technology, applied in the production of sugar, sugar products, sucrose production, etc., can solve the problems of energy waste, low production efficiency, waste of energy, etc., and achieve significant economic benefits, save labor costs, and reduce production costs. Effect

Active Publication Date: 2016-03-23
JIANGSU JIUWU HITECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, the existing production of refined sugar adopts the original process of lime precipitation and sulfur bleaching
This method has the following disadvantages: First, the plate and frame filter press is used, which is a relatively traditional, relatively low degree of automation, and labor-intensive equipment. Removing impurities such as colloids and tannins in the syrup will bring a large production load to the subsequent process sections; secondly, the use of lime precipitation technology will generate a large amount of residues, which will seriously pollute the environment. A new impurity --- ash is introduced into the process, resulting in lower product quality; third, the decolorization of this process is the use of sulfur fumigation, there will be sulfur residues in the product, which is harmful to human health, and the sugar bleached by sulfur dioxide will not be stored for a long time. Chromatography will occur after
With the further improvement of the country's food safety requirements, this method will be restricted in use; fourth, without using ion exchange desalination, the residual salt in the sugar solution cannot be removed, resulting in high ash content of the product, low quality or unqualified, Fourth, the traditional three-effect evaporator is used, which wastes a lot of energy. Compared with advanced technologies such as MVR, the energy consumption is higher
Fifth, the relevant process parameters have not been optimized, resulting in waste of energy

Method used

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  • Process and device for two-step sugar production
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] A kind of novel technology of sucrose production, it comprises the following steps:

[0033]A. Sugar: Add water and heat to 80°C to dissolve the raw sugar to make syrup. The sucrose content is about 40%, 50%, 60%, 70%, and 80% respectively;

[0034] B. Pretreatment: The syrup is pretreated through the plate frame to remove colloid or larger granular impurities; the accuracy of the plate frame filter cloth used is 0.1 μm;

[0035] C. Ceramic membrane filtration: the collected pretreated syrup is micro-filtered through a ceramic membrane, the average pore size is 50nm, the filtration temperature is 50°C, and the filtration pressure is 0.5Mpa to obtain the syrup clear liquid;

[0036] D. Primary ion-exchange desalination: Use macroporous strong basic anion-exchange resin for ion-exchange desalination of the syrup clear liquid, which can also play a role in decolorization. The flow rate in the resin column is 2BV / h, and the temperature is 70°C. The diameter-to-height ratio...

Embodiment 2

[0045] A kind of novel technology of sucrose production, it comprises the following steps:

[0046] A. Melting sugar: add water and heat to 80°C to dissolve the raw sugar to make a syrup, and the sucrose content is about 60% respectively;

[0047] B. Pretreatment: The syrup is pretreated through the plate frame to remove colloid or larger granular impurities; the accuracy of the plate frame filter cloth used is 5 μm;

[0048] C. Ceramic membrane filtration: the collected pretreated syrup is microfiltered through a ceramic membrane, the average pore size is 50nm, 200nm and 500nm respectively, the temperature of filtration is 90°C, and the filtration pressure is 0.1Mpa to obtain the syrup clear liquid;

[0049] D. Primary ion-exchange desalination: Use macroporous strong basic anion-exchange resin for ion-exchange desalination and decolorization of the syrup clear liquid. The flow rate in the resin column is 10BV / h, the temperature is 40°C, and the diameter-to-height ratio is 1 / ...

Embodiment 3

[0058] A kind of novel technology of sucrose production, it comprises the following steps:

[0059] A. Melting sugar: add water and heat to 80°C to dissolve the raw sugar to make a syrup, and the sucrose content is about 60% respectively;

[0060] B. Pretreatment: The syrup is pretreated through the plate frame to remove colloid or larger granular impurities; the accuracy of the plate frame filter cloth used is 4 μm;

[0061] C. Ceramic membrane filtration: The collected pretreated syrup is micro-filtered through a ceramic membrane, the average pore size is 200nm, the filtration temperatures are 50°C, 70°C, and 90°C, and the filtration pressure is 0.4Mpa to obtain clear syrup. liquid;

[0062] D. One-stage ion exchange desalination: The syrup clear liquid is desalted and decolorized by ion exchange with macroporous strong basic anion exchange resin. The flow rate in the resin column is 4BV / h, the temperature is 60°C, and the diameter-to-height ratio is 1 / 8 , the Brix of the ...

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Abstract

The invention discloses a process for preparing sugar by a two-step method and a device thereof. The process comprises the following steps: adding water into crude sugar for dissolving to obtain crude syrup; feeding the crude syrup into a primary filter and a micro-filtration membrane in sequence for filtering to obtain filtrate; feeding the filtrate into a first ion exchange resin tower to obtain a first penetrating fluid, wherein the first ion exchange resin refers to macroporous strong-basicity anion exchange resin; feeding the first penetrating fluid into a second ion exchange resin tower to obtain a second penetrating fluid, wherein the second ion exchange resin refers to strong-acidity cation exchange resin, weak-acidity cation exchange resin or a mixing bed of anion and cation exchange resin; feeding the second penetrating fluid into an evaporator for concentrating to obtain sucrose concentrated liquor; and crystallizing, centrifuging and drying to obtain a sucrose finished product. The process disclosed by the invention can be used for producing high-purity refined sucrose in batch, wherein a pigment removal rate reaches 99.9%, a salt removal rate reaches 98%, and sucrose component of the product reaches 99.9% which reaches the standard of national senior sugar.

Description

technical field [0001] The invention relates to a process and device for two-step sugar production, belonging to the technical field of sugar production. Background technique [0002] The sugar production in most developed countries in the world adopts the "two-step" sugar production method. Most sugar factories produce raw sugar, which is then supplied to refineries to produce refined sugar. The "two-step method" sugar production means that the sugar material first uses a relatively simple process (lime method) to produce raw sugar (that is, rough sugar), and then dissolves it, and recrystallizes it after purification to produce white sugar. A kind of white granulated sugar with high index requirements, higher color value, lower color value, and fewer impurities), in decolorization and desalination, it needs to be treated by ion exchange and other aspects. The main advantage of the "two-step method" is that after secondary clarification to remove impurities and secondary ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C13B50/00
Inventor 彭文博凌国庆张宇江健张宏
Owner JIANGSU JIUWU HITECH
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