Organic light-emitting device and preparation method thereof
An electroluminescent device, an organic technology, applied in the direction of electric solid-state devices, semiconductor/solid-state device manufacturing, electrical components, etc.
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[0069] On the other hand, the present invention provides a method for preparing an organic electroluminescent device, which includes the following steps:
[0070] Preparation of functional layer, light-emitting layer and cathode on the anode substrate;
[0071] The organic material film layer is vapor-deposited on the surface of the cathode by vacuum evaporation, and then the thermal buffer layer and the inorganic material film layer are sequentially prepared on the organic material film layer by magnetron sputtering, and finally the inorganic material film layer is prepared on the organic material film layer. A polyethylene terephthalate film layer is arranged on the surface of the material film layer to form an encapsulation layer;
[0072] Coat the edge of the polyethylene terephthalate film with ultraviolet glue, dry and harden the ultraviolet glue by ultraviolet curing, seal to form a closed space, and house the functional layer, the light-emitting layer and the cathode in the ...
Example Embodiment
[0096] Example 1
[0097] A method for preparing an organic electroluminescent device includes the following steps:
[0098] (1) Preparation of functional layer, light-emitting layer and cathode on the anode substrate
[0099] a. Pretreatment of conductive glass substrate
[0100] Take the ITO glass substrate and perform acetone cleaning → ethanol cleaning → deionized water cleaning → ethanol cleaning, all are cleaned with an ultrasonic cleaning machine, and the single washing is cleaned for 5 minutes, and then dried with nitrogen, and the oven is dried for use; The latter ITO glass undergoes surface activation treatment to increase the oxygen content of the conductive surface layer and improve the work function of the conductive layer surface; the thickness of ITO is 100nm;
[0101] b. Preparation of functional layer, light-emitting layer and cathode
[0102] The method of vacuum evaporation is used to sequentially form a hole injection layer, a hole transport layer, a light emitting l...
Example Embodiment
[0118] Example 2
[0119] A method for preparing an organic electroluminescent device includes the following steps:
[0120] (1) Preparation of functional layer, light-emitting layer and cathode on the anode substrate
[0121] Same as Example One;
[0122] (2) Prepare the encapsulation layer on the cathode
[0123] A 250nm NPB film is prepared on the surface of the cathode by vacuum evaporation as the organic material film layer, and the vacuum degree is controlled to 5×10 -5 Pa, the evaporation rate is
[0124] On the surface of the NPB film, a thermal buffer layer with a thickness of 120nm is prepared by magnetron sputtering, and SiO 2 As a target, the background vacuum is controlled to 5×10 -5 Pa, pass argon gas, flow rate is 8sccm;
[0125] In SiO 2 Magnetron sputtering is used to prepare an inorganic material film with a thickness of 100nm on the surface of the thermal buffer layer, using MoO 3 And SiO as the target material, the mass ratio of SiO is 30%, and the background vacuum d...
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