Leaching method of nickel cobalt lithium manganate waste battery positive-negative electrode mixed material
A technology of nickel-cobalt lithium manganate and mixed materials is applied in the field of leaching of positive and negative electrode mixed materials of nickel-cobalt lithium manganate waste batteries, which can solve the problems of industrial pure oxygen storage, transportation and use, and industrial pure oxygen is uneconomical for self-use. The problems such as the small amount of industrial pure oxygen can achieve obvious economic and environmental benefits, reduce pollution control costs, and improve the effect of metal leaching rate.
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Embodiment 1
[0025] Example 1: Mix 100g of nickel-cobalt lithium manganate waste battery positive and negative electrode mixed materials (containing 14.5% nickel, 20.3% cobalt, 17.5% lithium, 2.2% aluminum, 2.5% copper, 12.9% manganese) and ≤1.5mm wheat straw powder 29g was added to a titanium-lined pressure reaction kettle with a volume of 2L, and 1650ml of a mixed acid solution with a sulfuric acid concentration of 1.5mol / L and a nitric acid concentration of 5g / L was added, and the leaching was carried out under closed stirring (stirring speed 80r / min) at 50℃~60℃ 4h, liquid-solid separation was carried out after leaching to obtain 1600ml of leaching solution (without leaching residue washing water). The leaching rates of nickel, cobalt, lithium, copper, aluminum and manganese were 99.2%, 99.0%, 99.1%, 98.5%, 99.0% and 99.0%, respectively (according to the nickel, cobalt, lithium entering the leaching solution and the leaching residue washing solution) , copper, aluminum and manganes...
Embodiment 2
[0026] Example 2: Mix 300g of nickel-cobalt lithium manganate waste battery positive and negative electrode mixed materials (containing 14.5% nickel, 20.3% cobalt, 17.5% lithium, 2.2% aluminum, 2.5% copper, 12.9% manganese) and ≤1.5mm wheat straw powder 105g was added to a titanium-lined pressure reaction kettle with a volume of 5L, 3000ml of mixed acid solution with a sulfuric acid concentration of 3mol / L and a nitric acid concentration of 10g / L was added, and leached for 2h at 70℃~80℃ with closed stirring (stirring speed 70r / min) , and liquid-solid separation is carried out after the leaching is completed to obtain 2800ml of leaching solution (excluding leaching residue washing water). The leaching rates of nickel, cobalt, lithium, copper, aluminum and manganese were 99.4%, 99.2%, 99.5%, 99.2%, 98.6% and 99.1%, respectively (according to the nickel, cobalt, lithium entering the leaching solution and the leaching residue washing solution) , copper, aluminum and manganese ...
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