A kind of preparation method of primer for addition type silicone potting glue
A technology of silicone potting glue and primer, applied in adhesives, coatings and other directions, can solve the problems of unsuitable porous surface, affecting reliability, reducing sealing and caulking effect, etc., to achieve excellent chemical stability, easy to use. Industrial production, excellent viscosity increasing effect
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Embodiment 1
[0061] Embodiment 1: This embodiment provides a primer for addition-type silicone potting adhesive, and its production method includes the following steps:
[0062] (1) Preparation of primer:
[0063] The primer can be mainly composed of four components, including the first to fourth components. Preferably, the first component is methylvinyl dichlorosilane (dichloro(methyl)(vinyl)silane), and the second component is The second component is methylphenyldichlorosilane, the third component is phenyltrichlorosilane, and the fourth component is hydrogen-rich containing siloxane. The production method is as follows :
[0064] Mix 17g of methylvinyldichlorosilane, 0.3094g of methylphenyldichlorosilane, 51.67g of phenyltrichlorosilane and 69g of xylene evenly. Then, 100 g of water and 150 g of xylene were added into a 250 ml four-necked flask, and the temperature was raised to 50° C. The mixed solution of the monomers was added dropwise to the four-neck flask at a uniform speed, an...
Embodiment 2
[0072] Embodiment 2: This embodiment provides a primer for addition-type silicone potting glue, and its production method includes the following steps:
[0073] (1) Preparation of primer:
[0074] In this example, except that the hydrogen content of the added high hydrogen-containing silicone oil is different from that of Example 1, the steps and conditions of the production method for preparing the primer are the same. The difference is that 3.51g of high hydrogen-containing silicone oil (hydrogen content 0.5-0.9%, viscosity 20-200mPa.s) is added in this example, wherein the ratio of silicon hydrogen group to silicon vinyl group content is 0.4-0.72.
[0075] The prepared primer is transparent, has a refractive index of 1.46-1.50, and a light transmittance of 96-99%.
[0076] (2) Preparation of silicone potting compound:
[0077] The steps and conditions of the production method for preparing the encapsulant in this example are the same as those in Example 1.
[0078] (3) A...
Embodiment 3
[0081] Embodiment 3: the present embodiment provides a kind of primer for addition type silicone potting glue, and its production method comprises the following steps:
[0082] (1) Preparation of primer:
[0083] In this example, except that the hydrogen content of the added high hydrogen-containing silicone oil is different from that of Example 1, the steps and conditions of the production method for preparing the primer are the same. The difference is that 3.51g of high hydrogen-containing silicone oil (hydrogen content 0.1-0.4%, viscosity 20-200mPa.s) is added in this embodiment, wherein the ratio of silicon hydrogen group to silicon vinyl group content is 0.08-0.32.
[0084] The prepared primer is transparent, has a refractive index of 1.46-1.50, and a light transmittance of 96-99%.
[0085] (2) Preparation of silicone potting compound:
[0086] The steps and conditions of the production method for preparing the encapsulant in this example are the same as those in Exampl...
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Abstract
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