Method for preparing low-density oil well cementation cement test block through titanium diboride ceramic beads

A technology of titanium diboride and ceramic microbeads is applied in the field of materials, which can solve problems such as the inability to meet the needs of deep high-temperature oil wells, and achieve the effects of controllable particle size, low production cost and high activity.

Inactive Publication Date: 2014-06-04
YUEYANG PENGCHENG TECH DEV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] Due to the gradual reduction of oil and gas resources in low-temperature oil wells on land, the development of low-temperature oil wells on land has gradually shifted from low-temperature oil wells on land to deep land and ocean deep layers. The traditional cementing material floating beads cannot meet the needs of deep high-temperature oil wells.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] (1) Preparation of titanium diboride ceramic closed-cell hollow microspheres ① Ingredients firing: mix titanium diboride powder with a particle size of 1-15 μm and titanium dihydride powder with a particle size of 5-15 μm in a weight ratio of 95t%: 5wt% After stirring evenly, press it into a billet and dry it, then fire it in a vacuum atmosphere furnace at 1700°C for 3 hours to obtain a sintered body of titanium diboride ceramic material, and process the sintered body of titanium diboride ceramic material into 10~ 15 μm microbeads, ② Liquid preparation: Take 78wt% of 10-15μm titanium diboride ceramic microbeads and 22 wt% of water, add light potassium sulfate foaming agent to the slurry, the concentration is 1g / L ④ Filtration: filter large particles and impurity removal; ⑤ Firing: High-pressure jet high-speed centrifugal rotary spray method is used to form microspheres, and the dehydration expansion temperature is 800°C in a vertical four-zone electric furnace, the dryin...

Embodiment 2

[0045] (1) Preparation of titanium diboride ceramic closed-cell hollow microspheres ① Ingredients firing: mix titanium diboride powder with a particle size of 20-35 μm and titanium dihydride powder with a particle size of 20-30 μm in a weight ratio of 96wt%: 4wt% After stirring evenly, press it into a billet and dry it, then fire it in a vacuum atmosphere furnace at 1800°C for 2.5 hours to obtain a sintered body of titanium diboride ceramic material, and process the sintered body of titanium diboride ceramic material into 20~ 25 μm microbeads ② Dosing: 20-25 μm titanium diboride ceramic microbeads 75 wt%: water 25 wt%, add light potassium sulfate foaming agent to the slurry, the concentration is 1.5g / L ④ Filtration: large particles and impurity removal; ⑤ Firing: High-pressure spraying and high-speed centrifugal rotary spraying method is used to form microspheres. The dehydration expansion temperature is 820°C, the drying and sintering temperature is 1500°C, and the surface mel...

Embodiment 3

[0059](1) Preparation of titanium diboride ceramic closed-cell hollow microspheres ①Batching and firing: mix titanium diboride powder with a particle size of 40-50 μm and titanium dihydride powder with a particle size of 35-45 μm in a weight ratio of 97wt%: 3wt% After stirring evenly, press it into a billet and dry it, then fire it in a vacuum atmosphere furnace at 1900°C for 2 hours to obtain a sintered body of titanium diboride ceramic material, and process the sintered body of titanium diboride ceramic material in a spheroidizing machine into 30~ 35 μm microbeads, ② Liquid preparation: 30-35 μm titanium diboride ceramic microbeads 80 wt%: water 20 wt%, add light potassium sulfate foaming agent to the slurry, the concentration is 2g / L ④ Filtration: large particles and impurity removal; ⑤Firing: adopt high-pressure jet high-speed centrifugal rotary spray method to form microspheres, dehydrate and expand at 850°C in a four-zone electric furnace, dry and sinter at 1600°C, surfac...

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PUM

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Abstract

The invention provides a method for preparing a low-density oil well cementation cement test block through titanium diboride ceramic beads. The method comprises the following steps: preparing hollow titanium diboride ceramic obturator beads, batching, mixing, stirring and mixing size, testing a mould, testing strength, uniformly mixing and stirring 40-50wt% of class G oil well cement, 10-15wt% of superfine cement with the particle size of 13 microns, 25-35wt% of hollow titanium diboride ceramic obturator beads with particle sizes of 5-50 microns, 5-7wt% of coal ash with loss on ignition of 1.1%, 1.5-2wt% of calcium oxide with purity of 99.9%, 0.5-1.0 wt% of sodium sulfate and 1-3wt% of micro-silicon, stirring and mixing size in an agitator in a water-cement ratio of 0.5-0.6 (W/C) for 40 seconds, pouring the mortar in a test mould, curing the mortar for 24 hours or 48 hours in a water bath curing box with a constant temperature of 52 DEG C, demoulding, soaking the test block in cold water for 1 hour, and performing a performance test.

Description

technical field [0001] The invention relates to a method for preparing a low-density oil well cementing cement test block with titanium diboride ceramic microspheres, and belongs to the field of material technology. Background technique [0002] At present, domestic oil well cementing lightening agent uses floating beads in fly ash, including sinking beads and floating beads in fly ash, and the density of sinking beads is 1.1 ~ 2.8g / cm 3 , between, and the content accounts for 30-70% of fly ash. Floating beads are glass beads in fly ash that are less dense than water. Floating beads mainly include aluminosilicate glass beads and porous carbon particles. Floating beads after removing carbon particles It mainly includes thin-walled aluminosilicate glass beads with smooth inner and outer surfaces and large volume. 0.5-1% of the total amount of ash, the aluminosilicate glass microspheres are hollow spheres, and the floating beads in the fly ash are when the coal powder is burne...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B28/00C04B14/02
Inventor 郭志东
Owner YUEYANG PENGCHENG TECH DEV
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