Method for separating and extracting fine particle Ta-Nb concentrate

A technology of fine-grained, tantalum-niobium ore, applied in solid separation, wet separation, chemical instruments and methods, etc., to achieve the effect of high grade, low yield and improved sorting conditions

Active Publication Date: 2014-06-18
YICHUN TANTALUM & NIOBIUM MINE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These roughing enrichment technologies have the disadvantages of low recovery rate and low enrichment ratio when recovering tantalum and niobium in fine-grained ore slime, resulting in waste of tantalum and niobium resources
[0004] The key problems in the prior art: First, in the gravity separation process of general fine-grained tantalum-niobium ore slime, the fine ore mainly composed of gangue minerals A large amount of mud covers the surface of tantalum-niobium minerals or is closely combined with tantalum-niobium minerals, which is difficult to separate from useful minerals. This is also the main reason for the low grade of tantalum-niobium concentrates in the separation of fine-grained tantalum-niobium ore slimes
[0005] For example, the Chinese patent application No. 201210374718 "a method for beneficiation of fine-grained tantalum-niobium ore" is an improvement on the basis of the existing beneficiation method , which pretreats the slime, and then adds various regulators such as sodium carbonate, inhibitor water glass, activator lead nitrate, benzohydroxamic acid, hydroxyamino acid and other chemical reagents to the pretreated slime, This method of adding a variety of chemical reagents in the process of beneficiation has the following problems: first, too many chemical reagents are added; , the impact on the environment is high, and the production cost is high

Method used

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specific Embodiment approach

[0022] detailed description: The present invention will be further described in detail below in combination with specific embodiments.

[0023] The method of the present invention generally comprises the following three steps:

[0024] (1) Pretreat the raw material of tantalum-niobium slime to meet the requirements, then add dispersant to the mixing tank to disperse the raw material slime, so that the fine slime with gangue minerals as the main component in the raw material and tantalum-niobium minerals are effectively separated;

[0025] (2) Add flocculant into the mixing tank to flocculate the dispersed fine slime; the target mineral of flocculation is: the slime mainly composed of gangue minerals. The main purpose of flocculation: first, to prevent the dispersed fine slime mainly composed of gangue minerals from covering the surface of tantalum and niobium minerals again; second, the false specific gravity of flocs obtained by flocculation is relatively smaller due to st...

Embodiment 1

[0036] The fine-grained slurry of a certain tantalum-niobium mine containing tantalum and niobium was pretreated by concentration and dehydration until the mass percentage concentration of the pulp was 21.2%. Sodium hexametaphosphate, stirred for 4 minutes; then, according to the same ratio of 1.2 grams per ton of raw ore into the dressing pulp 1, add flocculant polyacrylamide, and stir for 4 minutes to get the dressing pulp 2; finally, 3300kg per hour into the dressing The flow of pulp 2 ore slime enters the LX-86 centrifugal concentrator for processing, and adopts a centrifugal acceleration of 100 m / s 2 to obtain fine tantalum and niobium concentrate products. The test index gained in the present embodiment is: raw ore grade (Ta, Nb) 2 o 5 0.0113%, tantalum and niobium concentrate grade (Ta, Nb) 2 o 5 0.152%, the yield rate of fine-grained tantalum-niobium concentrate is 3.64%, the recovery rate of fine-grained tantalum-niobium concentrate is 48.83%, and the enrichment ra...

Embodiment 2

[0037] Example 2. Except that all the other are identical with the explanation of embodiment 1 in the present embodiment except following explanation;

[0038] Pretreat a certain tantalum-niobium ore fine-grained slurry containing tantalum-niobium minerals until the pulp mass percentage concentration is 24.8%, add 14 grams of dispersant sodium hexametaphosphate per ton of dressing pulp, and stir for 5 minutes . Thereafter, according to the ratio of 1.1 g per ton of dressing pulp, add flocculant polyacrylamide and stir for 4 minutes. Finally, the ore-dressing slurry 1 enters the LX-86 centrifugal concentrator for processing at an ore-feeding flow rate of 3100 kg per hour, and adopts a centrifugal acceleration of 150 m / s to obtain fine-grained tantalum-niobium concentrates. The test indicators obtained in this embodiment are: Raw ore grade (Ta, Nb) 2 o 5 0.0114%, grade of tantalum and niobium concentrate (Ta, Nb) 2 o 5 0.148%, the yield rate of fine-grained tantalum-niobi...

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Abstract

The invention provides a method for separating and extracting fine particle Ta-Nb concentrate. Ta-Nb slurry is used as a raw material. The method comprises the steps of (1) pretreatment; (2) dispersion flocculation; (3) centrifugal grading selection; the pretreatment (1) comprises the steps of treating the Ta-Nb slurry till that the mass percentage is not lower than 20% as selection ore pulp 1; the dispersion flocculation (2) comprises the steps of adding a dispersant hexametaphosphate into the selection ore pulp 1, stirring for plural minutes, then adding a flocculant and stirring for plural minutes to obtain selection ore pulp 2; the centrifugal grading (3) comprises the steps of placing the selection ore pulp into a centrifugal separator for centrifugal grading so as to obtain the fine particle Ta-Nb concentrate. According to the method, the grade of the recycled fine particle Ta-Nb concrete is high, the recycle rate of the Ta-Nb concrete is high, the economic technical benefits are obvious, the treatment to three wastes is small, and the influence on the environment is small.

Description

Technical field: [0001] The invention relates to a method for separating and extracting tantalum-niobium concentrate, in particular to a method for separating and extracting fine-grained tantalum-niobium concentrate. Background technique : [0002] Tantalum and niobium are two important rare metal element materials, which have important strategic and economic value. With the development of economy, the consumption of various electronic products continues to grow, which makes the industrial demand for tantalum and niobium increase sharply, which intensifies the demand for tantalum and niobium. , The tightness of the supply of niobium mineral resources. my country has rich reserves of tantalum and niobium raw materials, of which tantalum accounts for 20% of the world's reserves, and niobium accounts for about 15% of the world's reserves. Fine, the recovery rate of beneficiation is low, especially the low recovery rate of tantalum and niobium in fine-grained ore slime is the ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B03B5/32B03B1/04
Inventor 丁勇毛美心王中明袁明才安占涛陈名瑞陈清李振飞丁婕
Owner YICHUN TANTALUM & NIOBIUM MINE
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