Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

A kind of preparation method of stainless steel surface silanization treatment film

A silanization treatment, stainless steel technology, applied in the direction of gaseous chemical plating, coating, metal material coating technology, etc., can solve the problems of stainless steel corrosion resistance to be improved, and achieve good corrosion resistance effect

Active Publication Date: 2016-08-17
北京优得泽科技有限公司
View PDF3 Cites 1 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, for gas samples containing acidic and corrosive substances, the acidic substances will react with the surface of the stainless steel tank wall during the storage of the sample, resulting in changes in the concentration of harmful substances in the gas sample. The surface of the stainless steel tank still needs further passivation treatment to improve corrosion resistance performance
Treating the surface of stainless steel by silanization method to improve the anti-corrosion performance of stainless steel surface has attracted people's attention, such as Chinese patents CN103087569 and CN103059625 respectively reported a silanization protective treatment agent and preparation method for the surface of anti-corrosion stainless steel plate, but by Corrosion resistance of stainless steel after silanization treatment needs to be improved

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Put the stainless steel tank that needs surface treatment into the chemical vapor deposition chamber, remove the water vapor on the surface of the stainless steel, evacuate the chemical vapor deposition chamber to vacuum, and then pass the mixed gas of silicon tetrahydride (99.9%) and phosphorus hydride (0.1%), and the gas phase The deposition pressure control range is 4Pa, the deposition temperature is 320°C, and the vapor deposition time is 2 hours. Chemical vapor deposition is carried out. After the deposition is completed, nitrogen gas is introduced and the temperature is lowered to room temperature. The thickness of the vapor-deposited amorphous silicon film on the surface of the stainless steel is 180 angstroms. The corrosion resistance of the stainless steel surface after silanization treatment reaches level 1, which has good corrosion resistance. The atmospheric collection samples containing corrosive substances are stored in stainless steel tanks for 72 hours. Sa...

Embodiment 2

[0025] Put the stainless steel tank that needs surface treatment into the chemical vapor deposition chamber, remove the water vapor on the surface of the stainless steel, evacuate the chemical vapor deposition chamber to a vacuum, and then pass the mixed gas of silicon tetrahydride (99.5%) and phosphorus hydride (0.5%), and the gas phase The deposition pressure control range is 100Pa, the deposition temperature is 410°C, and the vapor deposition time is 4.5 hours. Chemical vapor deposition is carried out. After the deposition is completed, nitrogen gas is introduced to cool down to room temperature. The thickness of the vapor-deposited amorphous silicon film on the surface of the stainless steel is 380 angstroms. The corrosion resistance of the stainless steel surface after silanization treatment reaches level 1, which has good corrosion resistance. The atmospheric collection samples containing corrosive substances are stored in stainless steel tanks for 72 hours. Sample concent...

Embodiment 3

[0027] Put the stainless steel tank that needs surface treatment into the chemical vapor deposition chamber, remove the water vapor on the surface of the stainless steel, evacuate the chemical vapor deposition chamber to a vacuum, and then pass the mixed gas of silicon tetrahydride (98.0%) and phosphorus hydride (2.0) into the gas phase deposition The gas pressure control range is 25Pa, the deposition temperature is 450°C, and the vapor deposition time is 6.8 hours. Chemical vapor deposition is carried out. After the deposition is completed, nitrogen gas is introduced and the temperature is lowered to room temperature. The thickness of the vapor-deposited amorphous silicon film on the surface of stainless steel is 650 angstroms. The corrosion resistance of the stainless steel surface after silanization treatment reaches level 1, which has good corrosion resistance. The atmospheric samples containing corrosive substances are stored in stainless steel tanks for 72 hours. Sample co...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
percent by volumeaaaaaaaaaa
percent by volumeaaaaaaaaaa
Login to View More

Abstract

The invention belongs to the technical field of material surface treatment, and discloses a preparation method of a stainless steel surface silanization treatment membrane. A amorphous silicon treatment membrane is formed on a stainless steel surface through chemical vapor deposition by adopting a mixed gas formed by silanization treatment agent silicon tetrahydride and doping agent phosphorus hydride, and the mixed gas contains 95%-99% by volume of silicon tetrahydride and 0.1%-0.5% by volume of phosphorus hydride. Compared with the prior art, the preparation method disclosed by the invention has the advantages that the stainless steel surface has good corrosion-resisting property after being subjected to silanization treatment and a gas sample which contains an acidic substance is not obviously changed in concentration in the process of being stored and transported in a stainless steel tank, thereby meeting the requirements for collection and analysis of the gas sample in an atmospheric environment.

Description

technical field [0001] The invention relates to the technical field of material surface treatment, in particular to a method for preparing a silanization treatment film on the surface of stainless steel. Background technique [0002] With the accelerated development of the industrialization process and the continuous strengthening of people's awareness of environmental protection, the pollution of harmful substances in the atmosphere to the environment has attracted more and more attention. Many harmful substances have pungent smells, even foul smells, which stimulate the sense of smell. Organs, causing people's unhappiness and damaging the living environment. Medical research has shown that harmful odors in the environment, especially stench, can affect human respiration, digestion, cardiovascular, endocrine and nervous systems. High concentrations of stench can also cause pulmonary edema or even suffocation to death. Long-term repeated stimulation by foul-smelling substan...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C23C16/24C23C16/52
Inventor 刘彦军曾建强
Owner 北京优得泽科技有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products