A kind of aluminum-lithium alloy material and its preparation method with improved vacuum melting process
A technology for aluminum-lithium alloys and alloy materials, which is applied in the field of preparation of aluminum-lithium alloy materials and their improved vacuum melting process, can solve the problems of low plasticity of aluminum-lithium alloys, achieve high alloy plasticity and toughness, prevent hydrogen absorption, and increase content Effect
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Embodiment 1
[0030] Embodiment 1 Preparation of aluminum-lithium alloy material of the present invention
[0031] Batching smelting: The raw materials are according to the mass ratio: lithium 2.0wt%, copper 0.03wt%, magnesium 5.0wt%, zirconium 0.1wt%, titanium 0.01wt%, iron 0.1wt%, silicon 0.05wt%, the balance is aluminum The ratio is put into the melting furnace, and the temperature of the melting furnace is controlled at 800° C. for 1.5 hours.
[0032] Detection: Spectroscopic analysis is used to detect the smelted alloy liquid to ensure that its composition is within the range.
[0033] Vacuum smelting: heat the alloy liquid to 700°C and place it in a vacuum melting furnace for remelting. Under the conditions of 700°C and 300Pa vacuum, vacuum smelt for 20 minutes.
[0034] Hydrogen absorption detection: through volumetric method, gravimetric method and other chemical methods to detect the hydrogen absorption of the alloy to be less than or equal to the mass fraction of 1×10 -7 .
[0...
Embodiment 2
[0042] Embodiment 2 Preparation of aluminum-lithium alloy material of the present invention
[0043] Batching smelting: the raw materials are according to the mass ratio: lithium 3.5wt%, copper 0.01wt%, magnesium 6.8wt%, zirconium 0.35wt%, titanium 0.1wt%, iron 0.2wt%, silicon 0.15wt%, the balance is aluminum The proportion is put into the smelting furnace, and the temperature of the smelting furnace is controlled at 850° C. for 1 hour.
[0044] Detection: Spectroscopic analysis is used to detect the smelted alloy liquid to ensure that its composition is within the range.
[0045] Vacuum smelting: heat the alloy liquid to 700°C and place it in a vacuum melting furnace for remelting. Under the conditions of 700°C and 500Pa vacuum, vacuum smelt for 20 minutes.
[0046] Hydrogen absorption detection: through volumetric method, gravimetric method and other chemical methods to detect the hydrogen absorption of the alloy to be less than or equal to the mass fraction of 1×10 -7 . ...
Embodiment 3
[0054] Embodiment 3 Preparation of aluminum-lithium alloy material of the present invention
[0055] Ingredients smelting: The raw materials are according to the mass ratio: lithium 2.75wt%, copper 0.02wt%, magnesium 7.5wt%, zirconium 0.275wt%, titanium 0.05wt%, iron 0.15wt%, silicon 0.1wt%, the balance is aluminum The ratio is put into the melting furnace, and the temperature of the melting furnace is controlled at 850° C. for 1.5 hours.
[0056] Detection: Spectroscopic analysis is used to detect the smelted alloy liquid to ensure that its composition is within the range.
[0057]Vacuum melting: heat the alloy liquid to 700°C and put it in a vacuum melting furnace for melting again. Under the conditions of 700°C temperature and 1000Pa vacuum degree, vacuum melting is carried out for 20 minutes.
[0058] Hydrogen absorption detection: through volumetric method, gravimetric method and other chemical methods to detect the hydrogen absorption of the alloy to be less than or equ...
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