Paint-indigo stereo overdyeing and fixation desizing-free sizing and dyeing process for jean blended warps
A desizing-free and denim-free technology, which is applied in the field of textile printing and dyeing, can solve the problems of indigo color fastness to be improved, weak three-dimensional sense or layering, desizing wastewater pollution, etc. Water performance for consistent results
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Embodiment 1
[0032] Prepare the self-crosslinking polyacrylate emulsion slurry (coating) containing blue paste FHYN (Zhuhai Yuchang Chemical Co., Ltd. provides) according to the method of invention patent embodiment 1 of publication number (CN103194917A), and the specific preparation method is:
[0033] Firstly, a transparent polyacrylate emulsion slurry without colorant was prepared according to the following formula (in parts by weight).
[0034]
[0035] Soft monomer butyl acrylate and methyl acrylate in the above-mentioned formula, hard monomer acrylic acid, methyl methacrylate and acrylonitrile, functional monomer methacrylate derivative HA, emulsifier (by weight ratio is 1: 1:2 composition of di-n-butyl sodium sulfosuccinate, disodium decyl polyoxyethylene ether sulfosuccinate and flat plus 0‐10) and 2 / 3 deionized water of the weight of the above formula are mixed at room temperature, The pre-emulsion was prepared by stirring for 20 min under the condition of 1000 r / min at a rotat...
Embodiment 2
[0050] Prepare the self-crosslinking polyacrylate emulsion slurry (coating) containing the scarlet pulp TRL (provided by Zhuhai Yuchang Chemical Co., Ltd.) according to the method of invention patent embodiment 2 of publication number (CN103194917A), and the specific preparation method is:
[0051]Firstly, a transparent polyacrylate emulsion slurry without colorant was prepared according to the following formula (in parts by weight).
[0052]
[0053]
[0054] Soft monomer, hard monomer, functional monomer and emulsifier in the above-mentioned formula (by weight ratio are 0.5:1:1.5 sodium di-n-butyl sulfosuccinate, decyl polyoxyethylene sulfosuccinate Disodium ester and flat plus 0‐10) and 2 / 3 of the above formula weight deionized water were mixed at room temperature and the rotation speed was 1000r / min and stirred for 20min to prepare a pre-emulsion; the initiator in the above formula was used in the formula 1 / 10 of the weight of deionized water in the reactor was disso...
Embodiment 3
[0067] According to the above-mentioned method of the invention patent embodiment 2 of the present application, firstly prepare a transparent self-crosslinking polyacrylate emulsion slurry without color paste, and then add the above-mentioned transparent self-crosslinking polyacrylate emulsion into the stirring tank , under the condition of stirring at a medium speed of 300r / min, in parts by weight, 1 part of lubricant (0.5 parts each of GWA-L and amphoteric silicone oil DC200, Shanghai Hongtai Chemical Co., Ltd.), 6 parts of paint color paste (Zhuhai City Yellow pulp (H10G) provided by Yuchang Chemical Co., Ltd., 0.05 part of defoamer (TEGO-810) and 0.2 part of thickener hydroxyethyl cellulose HEC were slowly added to the above self-crosslinking polyacrylate emulsion in sequence, and stirred for 0.5 After one hour, it was discharged, filtered, and packaged to obtain a self-crosslinking polyacrylate emulsion slurry containing yellow slurry H10G (provided by Zhuhai Yuchang Chemi...
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