A kind of preparation method of wc-co-cbn composite material
A composite material, wc-co-cbn technology, is applied in the field of preparation of WC-Co-cBN composite materials, and achieves the effects of low sintering temperature, low energy consumption and short sintering time
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Embodiment 1
[0026] (1) First weigh WC, metal Co powder and cBN raw materials in proportion, the mass ratio of WC and metal Co is 94:6, cBN accounts for 3% of the raw material volume fraction, and after uniform mixing, the mixture is mixed by ball milling, and the ball milling medium is Water ethanol, balls are Al 2 o 3 Balls, the ball milling time is 20 hours, and the mixing speed is 250 rpm;
[0027] (2) Dry the raw materials mixed by ball milling in an oven at 100°C, and then pass through a 200-mesh sieve before use;
[0028] (3) After putting the dried raw materials into the mold, place them in a hot-press sintering furnace. The sintering furnace heats up to 1280°C at a speed of 50°C / min, and keeps the temperature for 15 minutes, and the pressure is kept at 30MPa to obtain WC-Co-cBN composite material.
[0029] Its SEM picture is as follows figure 1 (a) and figure 2 As shown, it can be seen from the figure that cBN is evenly distributed on the cemented carbide substrate, and the...
Embodiment 2
[0032] (1) First weigh WC, metal Co powder and cBN raw materials in proportion, the mass ratio of WC and metal Co is 97:3, cBN accounts for 5% of the raw material volume fraction, and use ball milling after uniform mixing. The ball milling medium is Water ethanol, balls are Al 2 o 3 Balls, the ball milling time is 15 hours, and the mixing speed is 350 rpm;
[0033] (2) Dry the raw materials mixed by ball milling in an oven at 50°C, and then pass through a 100-mesh sieve before use;
[0034] (3) After putting the dried raw materials into the mold, place them in a hot-press sintering furnace. The sintering furnace is heated up to 1200°C at a speed of 30°C / min, and kept for 30 minutes, and the pressure is kept at 50MPa to obtain WC-Co-cBN composite material.
[0035] Its SEM picture is as follows figure 1As shown in (b), it can be seen from the figure that the cBN is evenly distributed on the cemented carbide substrate, and the cBN in the plan view is polygonal, indicating t...
Embodiment 3
[0038] (1) First weigh WC, metal Co powder and cBN raw materials in proportion, the mass ratio of WC and metal Co is 90:10, cBN accounts for 7% of the raw material volume fraction, and after uniform mixing, ball milling is used for mixing, and the ball milling medium is Water ethanol, balls are Al 2 o 3 Balls, the ball milling time is 18 hours, and the mixing speed is 150 rpm;
[0039] (2) Dry the raw materials mixed by ball milling in an oven at 200°C, and then pass through a 300-mesh sieve before use;
[0040] (3) After putting the dried raw materials into the mold, place them in a hot-press sintering furnace. The sintering furnace heats up to 1300°C at a speed of 40°C / min, and keeps the temperature for 5 minutes. The pressure is kept at 20MPa to obtain WC-Co-cBN composite material.
[0041] Its SEM picture is as follows figure 1 (c) and figure 2 It can be seen from the figure that cBN is evenly distributed on the cemented carbide substrate, and the content of cBN gra...
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