Preparation method for synthesizing anti-inflammatory decapeptide by using solid-phase polypeptide
A solid-phase peptide synthesis, anti-inflammatory decapeptide technology, applied in the preparation methods of peptides, chemical instruments and methods, peptides and other directions, can solve problems such as difficulties in peptide synthesis, and achieve the effects of stable process, stable quality and short production cycle
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[0078] Example 1
[0079] The examples and the list of raw materials used in the foregoing process are as follows:
[0080] No Name manufacturer 1 Rink Amide MBHA resin Tianjin Hecheng Technology Co., Ltd. 2 Fmoc-D-Tyr(tBu)-OH Suzhou Tianma Pharmaceutical Group 3 Fmoc-D-Arg(Pbf)-OH Suzhou Tianma Pharmaceutical Group 4 Fmoc-Gly-OH Suzhou Tianma Pharmaceutical Group 5 Fmoc-D-Nle-OH Suzhou Tianma Pharmaceutical Group 6 Boc-D-Arg-OH Suzhou Tianma Pharmaceutical Group 7 1-hydroxy-7-azobenzotriazole (HOAt) Suzhou Tianma Pharmaceutical Group 8 Benzotriazole-N,N,N',N'-tetramethylurea hexafluorophosphate (HBTU) Suzhou Tianma Pharmaceutical Group 9 N,N-Diisopropylethylamine (DIPEA) Sinopharm Chemical Reagent Co., Ltd. 10 Dimethylformamide (DMF) Sinopharm Chemical Reagent Co., Ltd. 11 Methanol Sinopharm Chemical Reagent Co., Ltd. 12 Hexahydropyridine (PIP) Sinopharm Chemical Reagent Co., Ltd. 13Mercaptoethanol (HOCH 2 CH 2 SH) Sinopharm Chemical Reagent Co., Ltd. 14 Triisopropylsilane (TI...
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