A preparation method of bismuth-based thin film with high tuning rate
A bismuth-based, high-profile technology, applied in ion implantation plating, metal material coating process, coating, etc., to achieve the effect of good crystallinity, orientation and tuning performance improvement
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Embodiment 1
[0027] (1) Clean the substrate substrate
[0028] Select a silicon substrate with a platinum electrode on the surface, place it in an alcoholic organic solvent for ultrasonic cleaning, rinse it with deionized water, and dry it in a nitrogen stream.
[0029] The substrate of the present invention may be a silicon substrate, an alumina substrate or a conductive glass substrate; the electrodes may be gold electrodes or platinum electrodes.
[0030] (2) Deposition induction layer
[0031] (a) Put the cleaned silicon substrate into the magnetron sputtering vacuum chamber, install the zinc bismuth niobate target on the corresponding radio frequency sputtering target, and start the vacuuming procedure.
[0032] (b) Wait until the vacuum degree reaches 9×10 -5 Torr, turn on the radio-frequency current source corresponding to the zinc-bismuth niobate target, pass in the working gas argon, complete radio-frequency magnetron sputtering, and prepare the zinc-bismuth niobate induction la...
Embodiment 2
[0041] The preparation process of Example 2 is the same as that of Example 1, except that the annealing temperature of the zinc-bismuth niobate induction layer is 650° C., and the tuning rate measured in Example 2 under the same conditions is 33%.
Embodiment 3
[0043] The preparation process of Example 3 is the same as that of Example 1, except that the annealing temperature of the zinc-bismuth niobate induction layer is 700° C., and the tuning rate measured in Example 2 under the same conditions is 31%.
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