Filter material and its manufacturing method
A technology of filter material and manufacturing method, applied in chemical instruments and methods, membrane, membrane technology, etc., can solve the problems of complicated manufacturing process of nano-ester fiber membrane and low performance of ion retention rate.
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preparation example Construction
[0025] The first solution can be prepared by dissolving the diamine compound in water, wherein the added amount of the diamine compound accounts for about 0.1-30% by weight of the first solution. The first solution may be further added with methanol, ethanol, isopropanol, or n-butanol. In addition, the second solution can be prepared by dissolving the acid chloride compound in an organic solvent, wherein the acid chloride compound accounts for about 0.1-1% by weight of the second solution, and the organic solvent used is such as n-hexane (hexane), trichlorotrifluoroethane 1,1,2-trichloro-1,2,2-trifluoroethane, pentane or heptane.
[0026] It should be noted that the polymer layer can be completely immersed in the first and second solutions. Therefore, after the interfacial polymerization reaction, the entire polymer layer can be converted into the surface selective composite layer to obtain figure 1 filter material shown. In addition, according to other embodiments of the p...
preparation example 1
[0031] Take 10g of sodium styrene sulfonate, 40g of 4-vinylpyridine, 7g of styrene, 50g of deionized water and 50g of isopropanol, put them into a reaction flask, and heat to 70°C under nitrogen. Take 0.2g potassium persulfate (KPS) as initiator and dissolve it in 10mL deionized water, inject it into the reaction bottle and continue to stir for 3 hours, then obtain ionic polymer (poly E) through precipitation and purification steps, the molecular weight is about 136784, and the product The rate is 88%.
[0032] Composite structure
preparation example 2
[0034] The ionic polymer (Poly E) obtained in Preparation Example 1 was dissolved in dimethylacetamide (DMAc) to obtain a solution (solid content: 18%). Next, the solution is formed on the support layer (PET non-woven fabric, thickness 110 μm) by discharge spinning to form a network polymer layer (thickness is about 10 μm, fiber diameter is between about 80 and 500 nm) to obtain a composite structure (1) .
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