Tea-seed oil extraction method with high oil yield
An extraction method and tea seed oil technology are applied in the field of tea seed oil extraction with high oil yield, which can solve the problems of low extraction rate, high content of harmful substances in tea seed oil, and few production equipment, and achieve good extraction effect and harmful effects. The effect of low material and increased material surface area
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Embodiment 1
[0015] A method for extracting tea seed oil with high oil yield, comprising the following process steps:
[0016] (1) Obtain tea seeds: take fresh pomegranate fruit, remove the pulp skin on the surface of the tea seeds, and then dry them in a vacuum freeze-drying oven, control the temperature of the cold trap at -32°C, and control the pressure at 19Pa, and dry for 2 hours;
[0017] (2) Superfine pulverization: Put the tea seeds dried in step (1) into an AO desktop miniature airflow pulverizer for coarse pulverization, and then put them into a miniature plant pulverizer for superfine pulverization, and pulverize The final tea seeds are sieved to obtain superfine tea seed powder, wherein the used sieve diameter is 7.5um.
[0018] (3) Extraction of tea seed oil: Add ethyl acetate-petroleum ether mixed extract with a solvent ratio of 1:6 to the superfine tea seed powder obtained in step (2), extract for 2 hours, and then place the extract In a rotary evaporator, control the e...
Embodiment 2
[0019] Example 2: The rest are the same as in Example 1, except that in the step (1), the temperature of the cold trap is controlled to be -35°C, the pressure is controlled to be 20 Pa, and the drying time is controlled to be 2.5h; in the step (2), the The diameter of the screen is 8um; in the step (3), the leaching time is 2.5, and the evaporation temperature is 45°C.
Embodiment 3
[0020] Example 3: The rest are the same as in Example 1, except that in the step (1), the temperature of the cold trap is controlled to be -37°C, the pressure is controlled to be 22 Pa, and the drying time is controlled to be 2.5h; in the step (2), the The diameter of the screen is 9um; in the step (3), the extraction time is 3 hours, and the evaporation temperature is 48°C.
[0021] After the above process steps, the tea seed oil sample is taken out to be tested:
[0022] serial number purity / % Extraction rate / % Moisture content / % Hazardous substance content / % Example 1 99 94.21 0.1 0.01 Example 2 99 93.58 0.2 0.02 Example 3 97 95.20 0.2 0.01
[0023] It can be seen from the above data that the purity of the produced tea seed oil sample is close to 100%, the purity is high, the extraction rate has reached more than 93%, the extraction rate is high, and the moisture content is low, the content of harmful substances is l...
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