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Tea-seed oil extraction method with high oil yield

An extraction method and tea seed oil technology are applied in the field of tea seed oil extraction with high oil yield, which can solve the problems of low extraction rate, high content of harmful substances in tea seed oil, and few production equipment, and achieve good extraction effect and harmful effects. The effect of low material and increased material surface area

Inactive Publication Date: 2014-11-19
ANHUI ZHONGSHENG EDIBLE OIL TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Tea seed oil is the main component of tea seeds, accounting for 25% to 35% of the dry weight of tea seeds. Tea seed oil refers to the general term for oils and fats extracted from the fruits (tea seeds) of camellia plants. It is a non-drying oil and is colorless. Or light yellow oily liquid, the physical and chemical properties are similar to the more expensive olive oil in the world, containing more than 70 kinds of palmitic acid, stearic acid, arachidic acid, palm oleic acid, oleic acid, linoleic acid, fat-soluble vitamins, etc. Composition, unsaturated fatty acid exceeds 80%, especially linoleic acid content as high as 20.6%, is a kind of edible vegetable oil with high nutritional value, application number is CN201210566347.3 discloses a kind of extraction method of tea seed oil, adopts flow Stated carbon dioxide extraction method, select the extraction pressure, extraction time, separation temperature, separation pressure as the main influencing factors, arrange the orthogonal experiment, take the extraction rate of tea seed oil as the test index, when the extraction pressure is 25MPa, the extraction time is 1h, the separation temperature is 25 ℃, and the separation pressure is 6MPa, and the tea seed oil product is obtained. This method has simple process and less production equipment. The method of extracting tea seed oil from tea seeds, the extracted tea The seed oil meets the national second-class edible oil standard, and the extraction method of tea seed oil has been opened up, but the extraction rate of this preparation method is low, and the content of harmful substances in the extracted tea seed oil is high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0015] A method for extracting tea seed oil with high oil yield, comprising the following process steps:

[0016] (1) Obtain tea seeds: take fresh pomegranate fruit, remove the pulp skin on the surface of the tea seeds, and then dry them in a vacuum freeze-drying oven, control the temperature of the cold trap at -32°C, and control the pressure at 19Pa, and dry for 2 hours;

[0017] (2) Superfine pulverization: Put the tea seeds dried in step (1) into an AO desktop miniature airflow pulverizer for coarse pulverization, and then put them into a miniature plant pulverizer for superfine pulverization, and pulverize The final tea seeds are sieved to obtain superfine tea seed powder, wherein the used sieve diameter is 7.5um.

[0018] (3) Extraction of tea seed oil: Add ethyl acetate-petroleum ether mixed extract with a solvent ratio of 1:6 to the superfine tea seed powder obtained in step (2), extract for 2 hours, and then place the extract In a rotary evaporator, control the e...

Embodiment 2

[0019] Example 2: The rest are the same as in Example 1, except that in the step (1), the temperature of the cold trap is controlled to be -35°C, the pressure is controlled to be 20 Pa, and the drying time is controlled to be 2.5h; in the step (2), the The diameter of the screen is 8um; in the step (3), the leaching time is 2.5, and the evaporation temperature is 45°C.

Embodiment 3

[0020] Example 3: The rest are the same as in Example 1, except that in the step (1), the temperature of the cold trap is controlled to be -37°C, the pressure is controlled to be 22 Pa, and the drying time is controlled to be 2.5h; in the step (2), the The diameter of the screen is 9um; in the step (3), the extraction time is 3 hours, and the evaporation temperature is 48°C.

[0021] After the above process steps, the tea seed oil sample is taken out to be tested:

[0022] serial number purity / % Extraction rate / % Moisture content / % Hazardous substance content / % Example 1 99 94.21 0.1 0.01 Example 2 99 93.58 0.2 0.02 Example 3 97 95.20 0.2 0.01

[0023] It can be seen from the above data that the purity of the produced tea seed oil sample is close to 100%, the purity is high, the extraction rate has reached more than 93%, the extraction rate is high, and the moisture content is low, the content of harmful substances is l...

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Abstract

The invention discloses a tea-seed oil extraction method with high oil yield, which belongs to the technical field of grease processing. The method comprises three procedures, i.e., acquirement of tea seeds, superfine grinding and extraction of tea-seed oil. According to the method, superfine grinding technology is employed, which is beneficial for extraction of tea-seed oil; an ethyl acetate-petroleum ether solvent is used as an extracting solution, so tea-seed oil yield is further improved; through strict control of parameters like temperature, pressure and time in acquirement of raw materials, the obtained tea seed raw materials have good quality, which is favorable for rapid extraction of tea-seed oil; in the process of extraction of tea-seed oil, maximization of oil yield is realized through controlling of extraction time; and compared with common processes, the method provided by the invention has an obvious better extraction effect, the content of harmful substances produced in preparation are extremely low, and a high safety coefficient is obtained.

Description

technical field [0001] The invention relates to the technical field of oil processing, in particular to a tea seed oil extraction method with high oil yield. Background technique [0002] Tea seed oil is the main component of tea seeds, accounting for 25% to 35% of the dry weight of tea seeds. Tea seed oil refers to the general term for oils and fats extracted from the fruits (tea seeds) of camellia plants. It is a non-drying oil and is colorless. Or light yellow oily liquid, the physical and chemical properties are similar to the more expensive olive oil in the world, containing more than 70 kinds of palmitic acid, stearic acid, arachidic acid, palm oleic acid, oleic acid, linoleic acid, fat-soluble vitamins, etc. Composition, unsaturated fatty acid exceeds 80%, especially linoleic acid content as high as 20.6%, is a kind of edible vegetable oil with high nutritional value, application number is CN201210566347.3 discloses a kind of extraction method of tea seed oil, adopts ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B1/04C11B1/10
Inventor 王庆彬
Owner ANHUI ZHONGSHENG EDIBLE OIL TECH
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