Method and apparatus for detecting membrane damage based on electrochemistry and magnetic bead technology

A detection device and detection method technology, applied in chemical instruments and methods, membrane technology, semi-permeable membrane separation and other directions, can solve the problems of insensitive detection, inability to online detection, small application range, etc., to achieve high detection sensitivity and improve production. Efficiency, wide application effect

Inactive Publication Date: 2014-11-26
JIANGSU UNIV
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  • Abstract
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Problems solved by technology

All of the above methods have their own defects. Although the turbidity detection method can be used for continuous on-line detection, the detection is not sensitive and is limited by the concentration of raw liquid particles and process conditions, so the application range is small.
Although the microbial tracer test method has high sensitivity, the biolo...

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  • Method and apparatus for detecting membrane damage based on electrochemistry and magnetic bead technology
  • Method and apparatus for detecting membrane damage based on electrochemistry and magnetic bead technology
  • Method and apparatus for detecting membrane damage based on electrochemistry and magnetic bead technology

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Embodiment Construction

[0020] see figure 1 , a membrane damage detection device based on electrochemical and magnetic bead technology of the present invention mainly includes: raw liquid tank 1, raw liquid feed pipeline 2, booster pump 3, concentrated liquid outlet pipe 7, clear liquid outlet pipe 9, membrane module 11 , magnetic bead detection device 12, clear liquid tank 15, etc. The feed liquid to be treated is packed in the stock solution tank 1, the center of the bottom of the stock solution tank 1 is connected to one end of the stock solution feed pipe 2, and the other end of the stock solution feed pipe 2 is connected to the upper end of the membrane module 11 through the stock solution feed pipe flange 5. The first valve 4 is set on the stock solution feed pipeline 2 near the bottom of the stock solution tank 1, the first valve 4 is used to control the circulation of the stock solution, and is installed on the stock solution feed pipe 2 between the first valve 4 and the membrane module 11 ...

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Abstract

The invention discloses a method and an apparatus for detecting membrane damage based on an electrochemistry and magnetic bead technology. According to the apparatus and the method, a horizontal segment at the exactly middle of a clear-liquid outlet pipe is provided with a magnetic-bead detection device tightly connected with the clear-liquid outlet pipe; a positive electrode sheet and a negative electrode sheet are horizontally arranged side by side along the radial direction at the middle part in a magnetic-bead detection pipe and are immersed in a clear liquid; the lower segments of two adjacent but contactless metal electrodes both stretch into the clear liquid in the magnetic-bead detection pipe, and the upper segments both stretch out of the magnetic-bead detection pipe and are both winded by a coil; the tops of the two metal electrodes are both connected with an MCU main control unit via an MCU sampling interface; the resistance R0 of the clear liquid is calculated out according to the voltage and the current; and magnetic beads with the diameter larger than the membrane aperture are added into the original liquid, the voltage between the two metal electrodes is acquired and the resistance R at the current moment is calculated out, the resistance R and the resistance R0 are compared, and the damage degree of a filtration membrane is characterized through variation of the resistance of the clear liquid. The detection sensitivity is high, and the membrane is not destroyed.

Description

technical field [0001] The invention relates to the technical field of detection of filter membrane damage, in particular to a membrane damage detection method and device based on electrochemical and magnetic bead technology. Background technique [0002] Membrane separation technology is required in industries such as biology, chemical industry, nuclear industry, metallurgy, food, beverage, medicine and environmental protection. In the process of membrane separation, the pore size of the membrane will change due to the repeated impact of the liquid, the corrosion of the membrane tube due to the precipitation of organic compounds, and the addition of filter-aided ultrasonic waves, which will cause membrane damage, and these damages are irreversible and irreparable. The removed impurities pass through the membrane and enter the clear liquid, and the extracted clear liquid contains impurities, which affects the filtration performance of the membrane. Therefore, how to timely...

Claims

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Application Information

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IPC IPC(8): B01D65/10
Inventor 张荣标王鹏孙健李文胜
Owner JIANGSU UNIV
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