A kind of nickel-molybdenum-aluminum rare earth coating and preparation method thereof
A nickel-molybdenum-aluminum and rare-earth technology, applied in the field of nickel-molybdenum-aluminum rare-earth coating and its preparation, can solve the problems of weak oxidation resistance and corrosion resistance, and achieve the effect of strong oxidation resistance and corrosion resistance.
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Embodiment 1
[0023] A nickel-molybdenum-aluminum rare earth coating is composed of four elements: nickel, molybdenum, aluminum and rare earth. Calculated by mass percentage, nickel: molybdenum: aluminum: rare earth is 53.90%: 33.68%: 9.00%: 3.42%.
[0024] The above-mentioned preparation method of a nickel-molybdenum-aluminum rare earth coating specifically comprises the following steps:
[0025] (1) Add 2.9g of nickel salt, 1.4g of molybdenum compound, 342g of aluminum salt, and 0.0978g of rare earth salt into 191g of ionic liquid, stir to dissolve, and obtain nickel salt-molybdenum compound-aluminum salt-rare earth salt-ionic liquid plating solution That is, nickel nitrate-molybdenum pentachloride-aluminum sulfate-cerium nitrate-1-ethyl-3-methyl-imidazolium bromide electroplating solution;
[0026] Wherein the ionic liquid is 1-ethyl-3-methyl-imidazolium bromide;
[0027] Wherein the nickel salt is nickel nitrate;
[0028] The molybdenum compound is molybdenum pentachloride;
[0029] ...
Embodiment 2
[0036] A nickel-molybdenum-aluminum rare earth coating is composed of four elements: nickel, molybdenum, aluminum and rare earth. Calculated by mass percentage, nickel: molybdenum: aluminum: rare earth is 19.47%: 42.83%: 18.50%: 19.20%.
[0037] The above-mentioned preparation method of a nickel-molybdenum-aluminum rare earth coating specifically comprises the following steps:
[0038] (1) Add 78g of nickel salt, 17.6g of molybdenum compound, 160g of aluminum salt, and 2.45g of rare earth salt into 198g of ionic liquid, stir and dissolve to obtain nickel salt-molybdenum compound-aluminum salt-rare earth salt-ionic liquid electroplating solution namely chlorine Nickel-nickel sulfate-ammonium molybdate-aluminum trichloride-lanthanum chloride-1-ethyl-3-methyl-imidazole tetrafluoroboric acid plating solution;
[0039] Wherein the ionic liquid is 1-ethyl-3-methyl-imidazolium tetrafluoroboric acid;
[0040] Wherein nickel salt is the mixture that nickel chloride and nickel sulfate ...
Embodiment 3
[0049] A nickel-molybdenum-aluminum rare earth coating is composed of four elements: nickel, molybdenum, aluminum and rare earth. Calculated by mass percentage, nickel: molybdenum: aluminum: rare earth is 33.86%: 35.12%: 14.5%: 16.52%.
[0050] The above-mentioned preparation method of a nickel-molybdenum-aluminum rare earth coating specifically comprises the following steps:
[0051] (1), 32.4g nickel salt, 10.89g molybdenum compound, 147g aluminum salt, 1.28g rare earth salt in 147g ionic liquid, stir and dissolve to obtain nickel salt-molybdenum compound-aluminum salt-rare earth salt-ionic liquid electroplating solution namely chlorine Nickel-sodium molybdate-aluminum trichloride-samarium chloride-1-ethyl-3-methyl-imidazolium chloride electroplating solution;
[0052] Wherein the ionic liquid is 1-ethyl-3-methyl-imidazolium chloride;
[0053] Wherein the nickel salt is nickel chloride;
[0054] The molybdenum compound is sodium molybdate;
[0055] Aluminum salt is aluminum...
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