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A kind of lycopene microcapsule particle and its preparation process

A technology of lycopene and granules, which is applied to the field of lycopene microcapsule granules and the preparation technology thereof, can solve the problems of poor fluidity, uneven material particles, and insufficient product particles, and achieves improved water solubility and palatability. , to avoid moisture absorption and adhesion, the effect of good cold water diffusion

Inactive Publication Date: 2017-03-22
武汉志邦化学技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For the selection of microcapsule coating materials, leather gelatin or animal gelatin is mostly used in traditional techniques. Although coating can also be completed to a certain extent, and the cost is relatively low, leather gelatin and animal gelatin often contain more Harmful substances such as cadmium, arsenic, and aflatoxin have been unable to meet the current product safety and hygiene standards
In addition, gelatin-coated products have poor fluidity and poor water solubility, especially not conducive to cold water diffusion and poor release, which greatly affects the use effect of the product
[0003] In addition, granulation spray is a commonly used technical method. Spray granulation inevitably involves product coating. The quality of the coating effect mainly depends on the coating material and drying technology. How to disperse the material particles as homogeneously as possible , complete heat and mass transfer in an instant, avoid material sticking or sticking to the wall, and complete drying is a technical problem faced in this field. The combination of spraying and drying technology in the traditional process is relatively simple, resulting in product coating. The stability is poor, and the product particles are not uniform enough
At present, most of the production equipment of lycopene microcapsules cannot be fully dried during the production process due to unreasonable structural design, resulting in defects such as uneven material particles and sticky particles, which affect the product. The quality and efficiency of continuous production, it is difficult to achieve effective recycling of coating components scattered in granulation, sieving, drying and other processes, resulting in a large waste of resources

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] (1) Add porous starch, natural VE oil and lycopene crystal powder to sunflower oil, dissolve it completely at a temperature of 35℃, and drain the oil. The drain pipe is filtered with a 120-mesh stainless steel screen, porous starch, natural VE oil, The weight ratio of lycopene solid powder and sunflower oil to porous starch: natural VE oil: lycopene crystal powder: sunflower oil is 0.5: 0.001: 0.5:1.

[0023] (2) Add purified water to the emulsification kettle, the weight ratio of purified water to lycopene crystal powder is 1:4.5, and the temperature of the jacket is increased by tapioca modified starch: corn syrup: trehalose: lycopene crystal powder as 0.5:3.0:0.5:1 weight ratio, feed modified cassava starch, corn syrup, trehalose, stir to completely dissolve, the temperature is controlled at 40℃; add the lycopene mixture to the emulsification kettle, the temperature in the emulsification kettle is 55°C , Measure the viscosity and control it at 30-60 centipoise, control ...

Embodiment 2

[0028] (1) Add porous starch, natural VE oil and lycopene crystal powder to corn oil, dissolve it completely at a temperature of 40℃, then drain the oil, filter the drain pipe with a 120-mesh stainless steel screen, porous starch, natural VE oil and tomato The weight ratio of red crystal powder and corn oil to porous starch: natural VE oil: lycopene crystal powder: corn oil is 1:0.01:3:4.

[0029] (2) Add purified water to the emulsification kettle, the ratio of purified water to lycopene crystal powder by weight is 1:5.0, while the temperature of the jacket is heated, the ratio by weight is converted into cassava modified starch: corn syrup: trehalose: tomato Red element crystal powder is 1:5.0:1.5:1, feed modified cassava starch, corn syrup, trehalose, stir to completely dissolve, temperature control at 50 ℃, add the lycopene mixture to the emulsification tank, the temperature in the emulsification tank is 55 ℃ , Measure the viscosity and control it at 30-60 centipoise, control...

Embodiment 3

[0034] (1) Add porous starch, natural VE oil and lycopene crystal powder to sunflower oil, dissolve it completely at a temperature of 45℃, and then drain the oil. The drain pipe is filtered with a 120-mesh stainless steel screen, porous starch, natural VE oil, The weight parts of lycopene solid powder and sunflower oil are 2:0.001:4:5 than porous starch: natural VE oil: lycopene crystal powder: sunflower oil;

[0035] (2) Add purified water to the emulsification kettle, the ratio of purified water to lycopene by weight is 1:5, while the jacket heats up, the ratio is converted into cassava modified starch by weight: corn syrup: trehalose: lycopene The crystal powder is 1.5:5.0:1:1, feed modified cassava starch, corn syrup, trehalose, stir to completely dissolve, temperature control at 50 ℃, add the lycopene mixture into the emulsification kettle, the temperature in the emulsification kettle is 58 ℃, measured The viscosity is controlled at 30-60 centipoise, the temperature is contr...

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PUM

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Abstract

The invention relates to lycopene microcapsule granules and a preparation process thereof. Lycopene crystal powder, sunflower oil or corn oil, porous starch, oxidized starch, modified cassava starch, corn syrup, trehalose, natural VE oil are used as main raw materials, a process is reasonably improved and optimized to be used for greatly shortening the production time, the entire production process is controlled, the drying is carried out layer by layer and the recycling is carried out step by step. Obtained products are spherical, the surfaces of the products are smooth and trim, the biological activity of the products is kept, the products can be well solved in cold water, the use, storage and transportation are relatively well facilitated, no organic solvent or harmful substance is left, the safety, liquidity, taste and water solubility of the products are greatly improved, and resource waste is reduced. By adopting the process, the yield of the lycopene microcapsule granules is high, and the process is suitable for being used for large scale preparation of the lycopene microcapsule granules, and is used for achieving the continuous mass production and reducing the production cost.

Description

Technical field [0001] The invention relates to the technical field of production of lycopene microcapsule particles, in particular to a lycopene microcapsule particle and a preparation process thereof. Background technique [0002] In the production process of lycopene microcapsule particles, spray drying and microcapsule coating are the two most critical technical steps, which directly affect the safety, fluidity, taste and water solubility of the product. Microcapsule wall material refers to the shell material used to coat the core material during microencapsulation, and is also called encapsulation material, capsule material, and shell material. Most of the materials that can be used as the wall material of the microcapsules are inert polymeric natural polymers, semi-synthetic polymers and synthetic polymer materials. Among them, natural polymer materials have the advantages of non-toxicity, good film-forming properties, and good stability. They are used in many applications...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A23P10/30A23L33/00A23L29/30A23L33/125A23P10/35
CPCA23L3/46A23V2002/00A23V2250/213
Inventor 何同胜关荣荣申永存
Owner 武汉志邦化学技术有限公司
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