Arc ion plating device for coating of inner wall of long pipe

A technology of arc ion plating and arc striking device, which is applied in ion implantation plating, sputtering plating, vacuum evaporation plating, etc., can solve corrosion, wear and high temperature oxidation, cannot meet the requirements of inner surface modification and strengthening, Problems such as limited depth of film deposition to achieve the effect of ensuring uniformity and quality

Inactive Publication Date: 2015-03-25
SHENYANG POLYTECHNIC UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] In the industry, the inner wall of a large number of metal workpieces needs to be modified, especially for long pipes or cylinders, such as pump cylinders of oil field pumps, petrochemical synthesis equipment, pipelines for oil and water transportation, especially for military use. Gun barrels and rocket tubes work under corrosion or high temperature, and are subjected to corrosion, wear and high temperature oxidation, or are affected by the above-mentioned multiple working conditions at the same time, and the current treatment methods cannot meet the requirements of such harsh environments. Internal Surface Modification and Strengthening Requirements
[0003] Compared with the outer surface of the component, the modification treatment of the inner wall of the pipe has the following technical problems: First, due to the limitation of the shape and size of the inner cavity, some treatment methods are difficult to implement, or even if it can be implemented, it is difficult to obtain a good improvement. Sexual effect, especially for long pipes with small diameter-to-length ratio
Second, limited by the shape and size of th

Method used

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  • Arc ion plating device for coating of inner wall of long pipe

Examples

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Effect test

Embodiment 1

[0019] Example 1: Depositing a metal titanium film layer on the inner surface of a stainless steel tube with a wall thickness of 1 mm in diameter and a length of Φ80×600 mm

[0020] Using a cylindrical target arc source with an outer diameter of 26mm, the hollow cylindrical cathode target is pure Ti, and a stainless steel tube with a wall thickness of 1mm and a diameter of Φ80×600mm is selected. Put it into the sample holder, the center line of the stainless steel tube coincides with the axis of the target arc source, and the moving speed of the sample holder is 2mm longitudinally and rotates one circle per minute. The vacuum chamber is evacuated to 6.7×10 -3 After Pa, Ar gas was introduced and the gas pressure in the vacuum chamber was maintained at 0.6Pa. First, the arc is ignited, the arc current is 60A, and the arc voltage is 20V. After the normal arc discharge, the sample holder starts to move, and the negative bias voltage of 900V is applied for bombardment cleaning for...

Embodiment 2

[0021] Example 2: Depositing a titanium nitride film layer on the inner surface of a stainless steel tube with a wall thickness of 1 mm in diameter and a length of Φ60×600 mm

[0022] Using a cylindrical target arc source with an outer diameter of 26mm, the hollow cylindrical cathode target is pure Ti, and a stainless steel tube with a wall thickness of 1mm and a diameter of Φ60×600mm is selected. Put it into the sample holder, the center line of the stainless steel tube coincides with the axis of the target arc source, and the moving speed of the sample holder is 2mm longitudinally and rotates one circle per minute. The vacuum chamber is evacuated to 6.7×10 -3 After Pa, Ar gas was introduced and the gas pressure in the vacuum chamber was maintained at 0.6Pa. First, the arc is ignited, the arc current is 60A, and the arc voltage is 20V. After the normal arc discharge, the sample holder starts to move, and the negative bias voltage of 900V is applied for bombardment cleaning f...

Embodiment 3

[0023] Example 3: A titanium nitride film was deposited on the inner surface of a stainless steel tube with a wall thickness of 1 mm in diameter and a length of Φ50×600 mm.

[0024] Using a cylindrical target arc source with an outer diameter of 26mm, the hollow cylindrical cathode target is pure Ti, and a stainless steel tube with a wall thickness of 1mm and a diameter of Φ50×600mm is selected. Put it into the sample holder, the center line of the stainless steel tube coincides with the axis of the target arc source, and the moving speed of the sample holder is 2mm longitudinally and rotates one circle per minute. The vacuum chamber is evacuated to 6.7×10-3 After Pa, Ar gas was introduced and the gas pressure in the vacuum chamber was maintained at 0.6Pa. First, the arc is ignited, the arc current is 60A, and the arc voltage is 20V. After the normal arc discharge, the sample holder starts to move, and the negative bias voltage of 900V is applied for bombardment cleaning for 3...

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Abstract

The invention relates to the field of preparation of a film and a coating, and particularly relates to a special arc ion plating cylindrical target arc source and an accessory part, which are used for depositing a film and a coating on the inner surface of the long pipe and the inner wall of a hole of a deep-hole device so as to realize a purpose of modifying the inner wall surfaces of military industrial and special parts. The arc ion plating device is characterized by being provided with a vacuum chamber, a cylindrical target arc source, an arc striking device, a sample rack for fixing the pipe, a circular gas homogenizing pipe, a sample rack heating system, a cathode target material and sample rack bias system, a vacuumizing system, a control cabinet, a cathode target power supply, a bias power supply and a worktable. The invention aims at providing the arc ion plating device for realizing the coating of the inner wall of the long pipe through the cylindrical target arc source and the accessory part, so that a purpose of protecting and modifying the inner surface of the long pipe and the inner wall of the hole of the deep-hole device can be realized.

Description

technical field [0001] The invention relates to the field of film and coating preparation, in particular to the development of a special arc ion plating columnar target arc source and accessory parts, which are used for depositing films and coatings on the inner surface of a long pipe and the inner wall of a deep hole device hole to realize The purpose of surface modification of inner wall of military and special parts. Background technique [0002] In the industry, there are a large number of inner walls of metal workpieces that need to be modified, especially for long pipe fittings or barrels, such as the pump barrel of oilfield oil pumps, petrochemical synthesis equipment, oil and water pipelines, especially those used in the military. Gun barrels and rocket tubes work under corrosion or high temperature, and are subject to corrosion, wear and high temperature oxidation, or are affected by the above-mentioned various working conditions at the same time. Internal surface ...

Claims

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Application Information

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IPC IPC(8): C23C14/32C23C14/50
Inventor 宋贵宏陈立佳杜昊迟松江肖金泉
Owner SHENYANG POLYTECHNIC UNIV
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