Nano silicon thermal insulation material and preparation method thereof

A thermal insulation material, nano-silicon technology, applied in chemical instruments and methods, layered products, ceramic layered products, etc., can solve the problems of inability to guarantee strength, affecting the use effect, and increasing thermal conductivity.

Active Publication Date: 2015-04-01
LUYANG ENERGY SAVING MATERIALS CO LTD
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  • Abstract
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  • Claims
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Problems solved by technology

Its anti-radiation layer only contains infrared opacifying agent and does not contain any reinforcing materials. Dry pressing cannot guarantee its strength and affect the use effect.
Moreover, although the addition of the anti-radiation layer can effectively suppress radiation heat transfer, the thermal conductivity of the components that make up the reinforcement layer and the anti-radiation layer are both large, and the thickness of the anti-radi

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  • Nano silicon thermal insulation material and preparation method thereof

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[0040] The invention also discloses a preparation method of nano silicon heat insulating material, comprising the following steps:

[0041] (A) uniformly mixing 60-80 parts by weight of nano silicon dioxide, 5-15 parts by weight of inorganic fibers and 15-35 parts of carbon black to obtain the first mixture;

[0042] Mix 60-80 parts by weight of nano silicon dioxide, 5-15 parts by weight of inorganic fibers and 15-35 parts of infrared light-shielding agent to obtain the second mixture; the infrared light-shielding agent is titanium dioxide, zirconium oxide, silicon carbide and hexatanium One or more of potassium phosphate whiskers;

[0043] (B) Put any one of the first mixture and the second mixture into the mold and scrape it, and then spread another mixture on the surface and scrape it, and then press to obtain the nano silicon heat insulating material.

[0044] The invention uses one or more of nano silicon dioxide, inorganic fiber, carbon black and titanium dioxide, zirco...

Embodiment 1

[0054] Weigh 60 parts by weight of nano-silica, 10 parts by weight of alkali-free glass fiber, and 30 parts by weight of carbon black, and slowly add each raw material into the nano-coating machine at the same time. After premixing at a low speed of 200rpm for 4 minutes, raise the rotor Rotate to 1000rpm, stir for 20min, after stirring, take out the material, and weigh 120g of the material into the mold as the bottom layer, use a scraper to scrape it; then weigh 60 parts by weight of nano-silica, 15 parts by weight of alkali-free Glass fiber, 25 parts by weight of silicon carbide, slowly add each raw material into the nano-coating machine at the same time, use the same mixing process to mix evenly, take out the material, weigh 120g of the material and spread it on the bottom material in the mold , use a scraper to scrape it flat, and then use a press with a pressure of 3.0MPa to compress the material to a thickness of 20mm and keep the pressure for 10min, and then demould to ob...

Embodiment 2

[0056] Weigh 75 parts by weight of nano-silica, 10 parts by weight of alumina fiber, and 15 parts by weight of carbon black, and slowly add each raw material into the nano-coating machine at the same time. After premixing at a low speed of 300 rpm for 4 minutes, increase the rotor speed of the nano-coating machine to 1200rpm, stirred for 15min, after the stirring was completed, the material was taken out, and 160g of the material was weighed and put into the mold as the bottom layer, and scraped with a scraper; then weighed 70 parts by weight of nano-silica, 15 parts by weight of alumina fiber 15 parts by weight of potassium hexatitanate whiskers, slowly add each raw material into the nano-coating machine at the same time, use the same mixing process to mix evenly, take out the material, and weigh 160g of the material and spread it on the bottom layer of the mold Use a scraper to scrape the top of the material flat, and then use a press with a pressure of 4.0MPa to compress the...

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Abstract

The invention provides a nano silicon thermal insulation material. The nano silicon thermal insulation material comprises a high temperature layer and a low temperature layer which is composited onto the high temperature layer; the low temperature layer consists of 60 to 80 parts by weight of nano silicon dioxide, 5 to 15 parts by weight of inorganic fibers and 15 to 35 parts of carbon black; the high temperature layer consists of 60 to 80 parts by weight of nano silicon dioxide, 5 to 15 parts by weight of inorganic fibers and 15 to 35 parts of an infrared shading agent; the infrared shading agent is one or more of titanium dioxide, zirconia, silicon carbide and potassium hexatitanate whisker. According to the nano silicon thermal insulation material, the effective extinction coefficient and the temperature resistance of different infrared shading agents of different types are adequately utilized, and the nano silicon thermal insulation material with ultralow heat conduction coefficient which can be used in a high temperature area can be prepared by utilizing different infrared shading agents of different types in a gradient manner.

Description

technical field [0001] The invention relates to the field of thermal insulation materials, in particular to nano silicon thermal insulation materials and a preparation method thereof. Background technique [0002] Traditional insulating refractory materials such as lightweight bricks, refractory fibers, and ceramic fiber blankets have relatively high thermal conductivity, and cannot meet the energy-saving requirements of industrial equipment with an outer wall temperature of less than 70 °C at a given thickness. Therefore, insulating materials with low thermal conductivity are becoming more and more popular. favored by people. In the early 1990s, A.J. Hunt and others first proposed the concept of super insulation materials, that is, insulation materials whose thermal conductivity is lower than that of "still air" under specific conditions of use. [0003] At present, there are two main types of super insulation materials: one is vacuum insulation materials, and the other is...

Claims

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Application Information

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IPC IPC(8): B32B18/00C04B30/02
CPCB32B18/00C04B30/02
Inventor 张成贺刘超任大贵张成
Owner LUYANG ENERGY SAVING MATERIALS CO LTD
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