Organic-inorganic composite water-based paint and preparation method thereof
A composite water-based and water-based paint technology, applied in the direction of coating, etc., can solve the problem of poor adhesion of nano-composite high-temperature fire-resistant coatings
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[0021] Correspondingly, the present invention also provides a preparation method of an organic-inorganic composite water-based paint, comprising the following steps: mixing iron powder, 1,3,5-trimesic acid, hydrofluoric acid, nitric acid and N,N-dimethyl Formamide is polymerized under hydrothermal conditions to obtain a metal-organic framework material; nano-titanium dioxide dispersion and talcum powder are added to the sodium silicate solution, and the metal-organic framework material and silica sol are added after the first stirring, Dispersant, leveling agent, defoamer, nonionic emulsion, styrene-acrylic emulsion, sodium acetate and water are stirred for the second time to obtain an organic-inorganic composite water-based paint.
[0022] As a preferred solution, in the step of obtaining the metal organic framework material, the temperature of the polymerization reaction is preferably 140-160° C., and the time of the polymerization reaction is preferably 8-20 hours. The conc...
Embodiment 1
[0039] Follow the steps below to prepare water-based paint:
[0040] 1. Contains the following components by weight: 32% of water (the first part of water: 12%, the second part of water 10%, the third part of water 10%), iron powder 3%, 1,3,5-benzenetri Acid 5%, hydrofluoric acid (35%) 0.1%, nitric acid (65%) 0.1%, N,N-dimethylformamide 0.5%, water-soluble sodium silicate 30%, silica sol 6%, non 0.3% ionic emulsion, 3% styrene-acrylic emulsion, nano TiO 2 Dispersion 5%, sodium acetate 0.15%, defoamer (organosiloxane) 0.3%, leveling agent (acetobutylcellulose) 0.15%, dispersant (polyacrylamide) 1.5%, talc 12%.
[0041] 2. Add iron powder, 1,3,5-trimesic acid, hydrofluoric acid (35%), nitric acid (65%), N,N-dimethylformamide and the first part of water into the reactor and mix well , put the lid on and move to the stainless steel reaction kettle to seal it, and place it in an electric blast drying oven at 150°C for 12 hours.
[0042] 3. Put the water-soluble sodium silicate s...
Embodiment 2
[0045] Follow the steps below to prepare water-based paint:
[0046] 1. Contains the following components by weight fraction: water 35% (the first part of water: 15%, the second part of water 10%, the third part of water 10%), iron powder 2%, 1,3,5-trimesic acid 4%, hydrofluoric acid (35%) 0.1%, nitric acid (65%) 0.1%, N,N-dimethylformamide 0.5%, water-soluble sodium silicate 35%, silica sol 8%, non-ionic Emulsion 0.3%, styrene-acrylic emulsion 5%, nano TiO 2 Dispersion 5%, sodium acetate 0.2%, defoamer (organosiloxane) 0.3%, leveling agent (acetobutylcellulose) 0.15%, dispersant (polyacrylamide) 1.5%, talc 12%.
[0047] 2. Add iron powder, 1,3,5-trimesic acid, hydrofluoric acid (35%), nitric acid (65%), N,N-dimethylformamide and the first part of water into the reactor and mix well , put the lid on and move to the stainless steel reaction kettle to seal it, and place it in an electric blast drying oven at 150°C for 12 hours.
[0048] 3. Put the water-soluble sodium silicat...
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