Continuous flow rotating shaft reactor and application thereof

Abstract

The invention discloses a continuous flow rotating shaft reactor, which comprises a power apparatus and a reactor body; the reactor body comprises a casing, a jacket and a rotating shaft, the jacket is arranged in the casing, the jacket is capable of encircling the rotating shaft, a chamber between the rotating shaft and the jacket is a reaction space; at least two material inlets and at least a products outlet which are communicated to the reaction space are arranged on the casing; at least a thermal medium inlet and at least a thermal medium outlet which are communicated to the jacket are arranged on the casing; and the rotating shaft is connected to the output shaft of the power apparatus. The continuous flow rotating shaft reactor can realize accurate control of temperature, full mixing and stirring of materials; and has the advantages of uniform mixing, high product purity, large yield, strong versatility, and simple structure and operation, and is especially suitable for a multiphase flow (gas-liquid, liquid-liquid, and gas-liquid-solid)reaction system of materials with characteristics of large ratio, large viscosity, easy precipitation and long standing time.

Description

technical field [0001] The invention relates to a continuous flow rotating shaft reactor and its application, in particular to a rotating shaft reactor capable of precise temperature control and sufficient mixing and stirring and its reaction in multiphase flow (gas-liquid, liquid-liquid, gas-liquid solid) system applications. It is especially suitable for multiphase flow reactions with large specificity, high viscosity, easy precipitation and long residence time, and belongs to the field of high gravity technology. Background technique [0002] Hypergravity technology is based on the gravity acceleration (9.8m / s) of the earth 2 ) A high-tech technology produced in a much larger environment. Rotating packed bed (i.e. supergravity machine, RPB) is the core equipment for realizing supergravity technology, and it is also a new type of equipment that enhances interphase mass transfer and multiphase mixing. As early as 1983, the British Imperial Chemical Industries Company suc...

AI Technical Summary

Problems solved by technology

For example, it is better to use a large-diameter, low-speed agitator for some operations; while another operation requires a small-diameter, fast paddle, which results in the need to replace different types of agitators when producing different products, resulting in cumbersome operations and poor versatility.

In the processing of some food or medicine, it is often necessary to add some additives to the mother liquor, and then stir and heat. In the whole process, the feeding, stirring and temperature have strict control parameters, and the existing equipment has high cost. , complex control and other issues, it is not suitable for small processing enterprises, especially those with limited operating places

In addition, the composition will also change during the cooling process of the product, which may affect the purity, particle size and distribution of the product, etc.

Most stirred tanks cannot evenly stir materials with high specific gravity, high viscosity, and easy precipitation, and cannot fully mix and react the materials, so that the production requirements cannot be met.

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