Method for examination of Sihuang dysentery-relieving particle quality
A technology for the quality of Sihuang Zhili Granules, which is applied in the field of quality inspection of Sihuang Zhili Granules, can solve the problems of no content measurement items and unfavorable quality, achieve good separation of main spots, improve quality level, and ensure product quality Effect
Inactive Publication Date: 2015-07-01
LUOYANG HUIZHONG ANIMAL MEDICINE
View PDF3 Cites 4 Cited by
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
[0005] "People's Republic of China Veterinary Pharmacopoeia" 2010 Edition, the quality standard of Sihuang Zhili Granules only identifies Coptidis Rhizome and Rheum Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhizoma Rhubarb in it, and there are no identification items for other medicines, and there is no content determination item, which is not conducive to controlling its quality. Clinical use is safe, effective and stable, it is necessary to establish a perfect quality inspection method
Method used
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View moreImage
Smart Image Click on the blue labels to locate them in the text.
Smart ImageViewing Examples
Examples
Experimental program
Comparison scheme
Effect test
Embodiment 1
[0039] 1. Identification of Scutellaria baicalensis Georgi:
[0040] Take 14g of the finely ground powder of this product, add 50ml of methanol, sonicate for 20 minutes, filter, evaporate the filtrate, add 2ml of methanol to the residue to dissolve, filter, and use the filtrate as the sample solution to be tested. Take another baicalin reference substance, add methanol to make a solution containing 1mg per 1ml, as the reference substance solution. According to thin layer chromatography (appendix page 32), draw 5μl of each of the above two solutions and place them on the same silica gel G plate with 4% sodium acetate and sodium carboxymethyl cellulose solution as the binder. Ester-butanone-formic acid-water (5:3:1:1) is used as the developing agent, placed in the exhibition tank for pre-saturation for 30 minutes, unfolded, taken out, dried, and sprayed with 1% ferric chloride ethanol solution. In the chromatogram of the sample to be tested, spots of the same color appear on the c...
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More PUM
| Property | Measurement | Unit |
|---|---|---|
| Concentration | aaaaa | aaaaa |
Login to View More
Abstract
The invention relates to a method for examination of Sihuang dysentery-relieving particle quality. The method is designed by proper improvement based on the original Sihuang dysentery-relieving particle standards and practical situation by product quality standard revision, adopts radix scutellariae identification and provides a berberine hydrochloride high performance liquid chromatography (HPLC) determination method. A methodology validation of the method proves that the method can effectively control product internal quality and guarantee product quality stability. The method has simple processes, satisfies traditional Chinese medicine product content determination requirements, controls active ingredient kinds as much as possible, improves a product quality level and improves market competitiveness.
Description
Technical field [0001] The invention belongs to the technical field of traditional Chinese medicine detection, and relates to a method for testing the quality of Sihuang Zhili granules. The method can be used for comprehensive evaluation of the quality of Sihuang Zhili granules. Background technique [0002] Sihuang Zhili Granules are made from 6 Chinese medicines of Coptis, Phellodendron, Rhubarb, Astragalus, Radix Isatidis, and Licorice after being extracted and processed into Sihuang Zhili extract, mixed with sucrose and dextrin in a certain proportion, and it has heat-clearing and laxative. The efficacy of fire and dysentery is mainly used for the treatment of damp-heat diarrhea and chicken colibacillosis, such as E. coli, Pasteurella, Salmonella infections in chickens and damp-heat diarrhea caused by secondary infections of viral diseases, white scour White dysentery, watery diarrhea, etc.; Swine E. coli, Salmonella caused diarrhea, yellow and white diarrhea, infectious gast...
Claims
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More Application Information
Patent Timeline
Login to View More IPC IPC(8): G01N30/90G01N30/02
Inventor 张许科刘兴金张晓会
Owner LUOYANG HUIZHONG ANIMAL MEDICINE