Application of potentilla anserine polysaccharide in preparation of hypoglycemic drugs or health products
The technology of fern hemp polysaccharide and health care product is applied in the application field of fern hemp polysaccharide in the preparation of hypoglycemic drugs or health care products, and can solve the problems of not lowering blood sugar in normal mice, lowering blood sugar, and having no statistical significance.
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Embodiment 1
[0024] The extraction of embodiment 1 ferns polysaccharide
[0025] Weigh the dried Junima, crush it, add about 8 times the amount of water, put it on the electric stove and cook for 1.5 hours, then filter the aqueous solution, repeat 3 times, combine the filtrates obtained from the 3 times, put them in an evaporating dish and evaporate and concentrate to 1: 1. Put the concentrated solution in a beaker, add 5 times the amount of 95% v / v ethanol, and let stand at low temperature overnight. Put the precipitate in a centrifuge tube and centrifuge (3000r / min, 10min), discard the supernatant, then add absolute ethanol, acetone, and ether to wash thoroughly, then centrifuge (3000r / min, 10min), discard the supernatant. The resulting precipitate was placed in a plate, and the gray powder obtained after the ether volatilized was Bracken polysaccharide, which was weighed. The yield was 2.66%.
Embodiment 2
[0026] Embodiment 2 Determination of the polysaccharide content of Bracken
[0027] The phenol-concentrated sulfuric acid method was used to determine the content of the polysaccharides in Bracken. Precisely draw 0.16, 0.20, 0.24, 0.28, 0.32, 0.36, 0.40mL of glucose standard solution, divide into 10mL volumetric flasks, add distilled water to dilute to the mark and mix well. Accurately pipette 2.0 mL into 10 mL test tubes with stoppers, and take another 2.0 mL of distilled water as a blank control. Add 1.0 mL of phenol solution to each tube, mix well, and quickly add concentrated H 2 SO 4 5.0mL, mixed and left for 5min, heated in a boiling water bath for 15min, taken out and cooled in cold water, measured absorbance at 490nm. The calculated regression equation is: y=0.042x-0.6836 R=0.9906.
[0028] Precisely weigh about 4mg of Juema polysaccharide in a 100ml volumetric flask, add water to dissolve and dilute to the scale, accurately draw 1.0ml and put it in a test tube, me...
Embodiment 3
[0029] The establishment of embodiment 3 diabetes mouse model
[0030] The experimental animals used were 110 male Kunming mice, weighing 17-23 g, provided by the Animal Experiment Center of Lanzhou University School of Medicine.
[0031] Take 110 clean-grade male Kunming mice weighing (20±3) g, 10 of which are the blank control group, and the remaining 100 are divided into cages, marked and weighed, and injected with 70 mg / kg of alloxan into the tail vein. Fasting blood glucose was measured after 3 days, and those with blood glucose value >11.1mmol / L were diabetic models.
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