Preparation method of artificial rutile
A technology of artificial rutile and acid-soluble titanium slag, which is applied to the removal of solid waste, titanium oxide/hydroxide, titanium dioxide, etc., can solve the problems of high investment cost, low quality of titanium-rich materials, and increase the difficulty of technical operation. Improved purity, improved efficiency, and easy leaching effects
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[0076] Example 1: Preparation of artificial rutile
[0077] The implementation steps of this embodiment are as follows:
[0078] A. Modification treatment
[0079] The acid-soluble titanium slag obtained from Panzhihua Iron and Steel Group Titanium Industry Co., Ltd. was analyzed by the method described in this manual. Its chemical composition is TiO by weight. 2 72.0%, SiO 2 9.5%, 1.5% MgO and 0.5% CaO; the particle size of the acid-soluble titanium slag is -100 mesh which is 80% by weight.
[0080] According to the weight ratio of acid-soluble titanium slag and modifier of 5:1.4, the acid-soluble titanium slag and sodium carbonate modifier were mixed uniformly, and then the microwave box reactor (HM Type) in the microwave reactor sold under the conditions of microwave reactor frequency of 912MHz and temperature of 780°C for 2.4 hours to obtain a modified acid-soluble titanium slag, which is tested by the method described in this manual. Chemical composition is Na 2 Fe 2 Ti 6 O 16...
Example Embodiment
[0085] Example 2: Preparation of artificial rutile
[0086] The implementation steps of this embodiment are as follows:
[0087] A. Modification treatment
[0088] The acid-soluble titanium slag obtained from Yunnan Xinli Nonferrous Metals Co., Ltd. was analyzed using the method described in this manual. Its chemical composition is TiO by weight. 2 72.5%, SiO 2 9.2%, MgO 1.2% and CaO 0.5%; the particle size of the acid-soluble titanium slag is -100 mesh, which is 80 86 82 84 84 83% by weight.
[0089] According to the weight ratio of acid-soluble titanium slag and modifier of 5:1.6, the acid-soluble titanium slag and sodium hydroxide modifier are mixed uniformly, and then the product is used in a microwave box reactor under the trade name of Kunming University of Science and Technology ( HM type) microwave reactor sold under the conditions of microwave reactor frequency of 915MHz and temperature of 800 ℃ modified treatment for 3.6 hours to obtain a modified acid-soluble titanium sla...
Example Embodiment
[0094] Example 3: Preparation of artificial rutile
[0095] The implementation steps of this embodiment are as follows:
[0096] A. Modification treatment
[0097] The acid-soluble titanium slag obtained by Yuntong Group Titanium Industry Co., Ltd. was analyzed by the method described in this manual. Its chemical composition is TiO by weight. 2 72.8%, SiO 2 9.0%, MgO 0.9% and CaO 0.2%; the particle size of the acid-soluble titanium slag is -100 mesh, which is 82% by weight.
[0098] According to the weight ratio of acid-soluble titanium slag and modifier of 5:1.0, mix the acid-soluble titanium slag with sodium carbonate, sodium hydroxide, phosphorus pentoxide, sodium phosphate or ammonium dihydrogen phosphate modifier uniformly , And then in a microwave reactor sold under the trade name microwave box reactor (HM type) by Kunming University of Science and Technology under the conditions of a microwave reactor frequency of 918MHz and a temperature of 750°C for 2.0h to obtain a Modifi...
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