Transparent wear-resistant super-hydrophobic coating material, preparation method and coating process thereof

A technology of super-hydrophobic coating and coating process, which is applied in the direction of polyester coating, epoxy resin coating, polyurea/polyurethane coating, etc., and can solve the problems of large-scale preparation and commercial application of transparent super-hydrophobic surface, and achieve Effects of enhancing wear resistance, improving durability, and enhancing bonding force

Active Publication Date: 2015-09-16
王舒
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, large-scale preparation and commercial application of transparent superhydrophobic surfaces have not yet been realized,

Method used

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  • Transparent wear-resistant super-hydrophobic coating material, preparation method and coating process thereof
  • Transparent wear-resistant super-hydrophobic coating material, preparation method and coating process thereof
  • Transparent wear-resistant super-hydrophobic coating material, preparation method and coating process thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] Paint preparation:

[0034] Add 0.5g Degussa Aerosil-R972 hydrophobic fumed silica (particle size: 20-100nm) to 500mL ethanol solution, stir evenly, put it into an ultrasonic cleaner (power 600W) and ultrasonically treat it for 10min to obtain nanomaterial dispersion liquid;

[0035] Under mechanical stirring (rotating speed 300 rpm), 50g elastic polyurethane colloidal particles Mix with a mixed solution of 300mL acetone and 200mL xylene and stir for 30min to obtain a binder material dispersion.

[0036] The transparent wear-resistant super-hydrophobic coating includes a nanometer material dispersion and a bonding material dispersion.

[0037] Coating process:

[0038] Clean the glass plate with pure water, spray the prepared bonding material dispersion on the glass plate (15*15cm 2 , thickness 15mm), the thickness is controlled at 0.5 μm, and then it is placed in a fume hood to dry for 30 minutes. After the drying is completed, the distance from the glass plate is...

Embodiment 2

[0041] Paint preparation:

[0042] Add 50g of Jibisheng HL-150 hydrophobic fumed silica (particle size: 20-100nm) to 500mL of isopropanol solution, stir evenly, put it into an ultrasonic cleaner (power 600W) for 90 minutes of ultrasonic treatment, and obtain nanomaterials Dispersions;

[0043] Under mechanical stirring (rotating speed 300 rpm), 50g elastic polyurethane After stirring with 500 mL of acetone solution for 30 min, 5 g of polypropylene (with a particle size of 100 μm) was added thereto, and the stirring was continued for 0.5 h to obtain a binder material dispersion.

[0044] The transparent wear-resistant super-hydrophobic coating includes a nanometer material dispersion and a bonding material dispersion.

[0045] Coating process:

[0046] Clean the glass plate with pure water, spray the prepared bonding material dispersion on the glass plate (15*15cm 2 , thickness 15mm), the thickness is controlled at 5 μm, and then it is placed in a fume hood to dry for 60 min...

Embodiment 3

[0049] Paint preparation:

[0050] Add 20g of hydrophobic nano-silica aerosol powder (particle size: 20-100nm) to 500mL ethanol solution, stir evenly, put it into an ultrasonic cleaner (power 600W) for ultrasonic treatment for 60min, then add 5g of chain nano-silica aerosol powder Silicon, put it into an ultrasonic cleaner (power 600W) and ultrasonically treat it for 1h to obtain a nanomaterial dispersion;

[0051] Under mechanical stirring (300 rpm) and a constant temperature water bath at 50°C, stir 25g of French Arkema 28-800EVA and 500mL of xylene solution for 90min to obtain a binder material dispersion.

[0052] The transparent wear-resistant super-hydrophobic coating includes a nanometer material dispersion and a bonding material dispersion.

[0053] Coating process:

[0054] Clean the cement board with lye, brush the prepared bonding material dispersion on the cement board (24*12cm 2 , thickness 25mm), the thickness is controlled at 10 μm, and then it is placed in a...

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Abstract

The present invention relates to a transparent wear-resistant super-hydrophobic coating material, a preparation method and a coating process thereof. The transparent wear-resistant super-hydrophobic coating material comprises a nanometer material dispersion liquid and an adhesion material dispersion liquid. According to the present invention, during the preparation, a nanometer material and a volatile solvent are mixed and dispersed to prepare the nanometer material dispersion liquid, and the adhesion material and the good solvent thereof are mixed and dispersed to prepare the adhesion material dispersion liquid; during the coating, the substrate surface is cleaned, the adhesion material dispersion liquid is coated to form the adhesion layer, the nanometer material dispersion liquid is coated after drying, the partial nanometer material is embedded into the adhesion layer through heating, pressurization and other ways, and finally the unstably-binding nanoparticles are removed by using scraping or adhesive tape adhesion to obtain the super-hydrophobic coating, wherein the coating has characteristics of good transparency, strong binding force, and wear resistance; and the super-hydrophobic coating material of the present invention can be used for the surfaces of a variety of materials such as metals, plastics, glass, cement boards and the like so as to achieve functions of water resistance, stain resistance, corrosion resistance, self-cleaning, dew resistance, icing resistance, and the like.

Description

technical field [0001] The invention belongs to the technical field of preparation and application of super-hydrophobic surfaces, and in particular relates to a transparent wear-resistant super-hydrophobic coating, a preparation method and a coating process thereof. Background technique [0002] The phenomenon of superhydrophobicity exists widely in nature, such as lotus leaves, butterfly wings, water strider legs, etc. all show excellent superhydrophobicity. The superhydrophobic coating is composed of a micro-nano-scale structure and a surface with low surface energy, and has the characteristics of a static contact angle of water greater than 150° and a rolling angle of less than 10°. Research on superhydrophobic surfaces has been one of the frontiers and hotspots of international scientific research in the past two decades. A breakthrough has been made. Common superhydrophobic structures such as ordered microcolumns, porous structures, nanowires, micronanoparticle cluste...

Claims

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Application Information

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IPC IPC(8): C09D175/04C09D123/08C09D125/06C09D127/12C09D183/04C09D161/06C09D163/00C09D167/08C09D7/12B05D5/08B05D3/02B05D3/04
Inventor 王舒王雯王蝶儿
Owner 王舒
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