Blue photosensitive resin composition, blue filter and display device having same
A resin composition, blue light-sensitive technology, applied in optical filters, photosensitive materials for optomechanical equipment, optics, etc., can solve problems such as visibility problems, difficulties in manufacturing high-quality display devices, pattern defects, etc., and achieve The effect of improving flatness
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preparation example 1
[0182] [Preparation Example 1]: Preparation of Pigment Dispersion Composition
[0183] 12.0 parts by weight of C.I. Pigment Blue 15:6 as a pigment, 4.0 parts by weight of DISPERBYK-2001 (purchased from BYK) as a pigment dispersant, and 84 parts by weight of propylene glycol methyl ether acetate as a solvent were carried out by using a ball mill. Mix / disperse for 12 hours to prepare a pigment dispersion composition.
[0184]
Synthetic example 1
[0185] Synthesis Example 1: Synthesis of Alkali-Soluble Resin
[0186] 120 parts by weight of propylene glycol monomethyl ether acetate, 80 parts by weight of propylene glycol monomethyl ether, 2 parts by weight of AIBN, 13.0 parts by weight of methacrylic acid, 10 parts by weight of benzyl methacrylate, 57 parts by weight of 4-Methylstyrene, 20 parts by weight of methyl methacrylate and 3 parts by weight of n-dodecyl mercaptan are put into a mixer, thermometer, reflux condenser, dropping liquid distributor (dropping lot) and Nitrogen was supplied to the flask in the tube, and the inside of the flask was purged with nitrogen. Thereafter, the resulting mixture was stirred, the temperature of the reaction mixture was raised to 110° C., and the reaction was performed for 6 hours, and thus an alkali-soluble resin was synthesized. The acid value of the solid of the alkali-soluble resin thus synthesized was 100.2 mgKOH / g, and its weight average molecular weight measured by gel perm...
Synthetic example 2
[0187] Synthesis Example 2: Synthesis of Alkali-Soluble Resin
[0188] 200 parts by weight of propylene glycol monomethyl ether acetate, 45 parts by weight of propylene glycol monomethyl ether, 4 parts by weight of azobisisobutyronitrile (AIBN), 15 parts by weight of acrylic acid, 70 parts by weight of benzyl methacrylate Esters, 15 parts by weight of styrene and 3 parts by weight of n-dodecylmercaptan were placed in a flask equipped with a stirrer, thermometer, reflux condenser, drop distributor and nitrogen supply tube, and purged with nitrogen The inside of the flask. Thereafter, the resulting mixture was stirred, the temperature of the reaction mixture was raised to 110° C., and the reaction was performed for 2 hours, and thus an alkali-soluble resin was synthesized. The acid value of the solid of the alkali-soluble resin thus synthesized was 110.4 mgKOH / g, and its weight-average molecular weight measured by GPC was about 8900.
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