Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

ITO film etching solution for liquid crystal panel manufacturing process and preparation method thereof

A manufacturing process and liquid crystal panel technology, applied in the direction of surface etching compositions, chemical instruments and methods, etc., can solve the problems of microcrystal residue, high transportation cost, easy crystallization, etc., to avoid unclean etching and improve etching effect , the effect of reducing surface tension

Active Publication Date: 2015-10-07
JIANGYIN JIANGHUA MICROELECTRONICS MATERIAL
View PDF4 Cites 3 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the ITO etching solution is mainly composed of oxalic acid crystals and pure water. This product mainly has the following disadvantages: ①The surface tension of the oxalic acid-type ITO etching solution used by domestic manufacturers is about 70mN / m, and the wettability of the ITO layer is insufficient. , resulting in residual microcrystals after etching; ②It is easy to crystallize when it is lower than 5°C, and it needs to be transported with heat preservation during transportation, and the transportation cost is high; at the same time, it is easy for customers to cause filter blockage when using it, which will affect customer equipment and use

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • ITO film etching solution for liquid crystal panel manufacturing process and preparation method thereof
  • ITO film etching solution for liquid crystal panel manufacturing process and preparation method thereof
  • ITO film etching solution for liquid crystal panel manufacturing process and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Embodiment 1, the present invention is a kind of ITO film etchant in liquid crystal panel manufacturing process, and it comprises the composition of following percentage by weight: oxalic acid 3.5%; Butyric acid 0.2%; N-valeric acid 1.2%; Iodic acid 1.2%; Hydrochloric acid 15%; the rest is pure water. Wherein, oxalic acid is the oxalic acid crystal of concentration greater than 99.5% (percentage by weight), the concentration of butyric acid is greater than 99.5% (percentage by weight), the concentration of n-valeric acid is greater than 89% (percentage by weight), and the concentration of iodic acid is greater than 79% (percentage by weight) Percent), the concentration of hydrochloric acid is greater than 55% (percentage by weight).

[0019] Taking the ITO film etching solution in the above liquid crystal panel manufacturing process as an example, the preparation process steps are as follows:

[0020] The first step: add the strong acidic cation exchange resin to hydro...

Embodiment 2

[0027] Embodiment 2, the present invention is a kind of ITO film etchant in liquid crystal panel manufacturing process, and it comprises the composition of following percentage by weight: oxalic acid 3.8%; Butyric acid 0.4%; N-valeric acid 1.6%; Iodic acid 1.6%; Hydrochloric acid 16%; the rest is pure water. Wherein, oxalic acid is oxalic acid crystal with a concentration greater than 99.5%, the concentration of butyric acid is greater than 99.5%, the concentration of n-valeric acid is greater than 89%, the concentration of iodic acid is greater than 79%, and the concentration of hydrochloric acid is greater than 55%.

[0028] Taking the ITO film etching solution in the above liquid crystal panel manufacturing process as an example, the preparation process steps are as follows:

[0029] The first step: add the strong acidic cation exchange resin to hydrochloric acid, stir and mix, the stirring speed is 65 rpm, and the stirring time is 8 minutes, then filter out the strong acid...

Embodiment 3

[0036] Embodiment 3, the present invention is a kind of ITO film etchant in liquid crystal panel manufacturing process, and it comprises the composition of following percentage by weight: oxalic acid 4.0%; Butyric acid 0.5%; N-valeric acid 2.0%; Iodic acid 2.0%; Hydrochloric acid 17%; the rest is pure water. Wherein, oxalic acid is oxalic acid crystal with a concentration greater than 99.5%, the concentration of butyric acid is greater than 99.5%, the concentration of n-valeric acid is greater than 89%, the concentration of iodic acid is greater than 79%, and the concentration of hydrochloric acid is greater than 55%.

[0037] Taking the ITO film etching solution in the above liquid crystal panel manufacturing process as an example, the preparation process steps are as follows:

[0038] The first step: add the strong acidic cation exchange resin to hydrochloric acid, stir and mix, the stirring speed is 68 rpm, and the stirring time is 8 minutes, then filter out the strong acid...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses an ITO film etching solution for a liquid crystal panel manufacturing process. The ITO film etching solution comprises, by weight, 3.5-4.3% of oxalic acid, 0.2-0.8% of butyric acid, 1.2-2.6% of n-pentanoic acid, 1.2-2.6% of iodic acid, 15-20% of hydrochloric acid and the balance pure water. Through use of additives such as butyric acid, n-pentanoic acid, iodic acid and hydrochloric acid based on the original technology, ITO etching solution surface tension is effectively reduced, penetration and infiltration effects are produced, an indium tin oxide semiconductor transparent conductive film etching rate is moderate and a reaction is stable so that product etching effects are improved without influence on product quality, the product can be stored at a low environment temperature, incomplete etching produced by the original technology is avoided, and storage at a low temperature is realized. The ITO film etching solution is suitable for large scale production.

Description

technical field [0001] The invention relates to an ITO film etching solution in a liquid crystal panel manufacturing process and a preparation method thereof. Background technique [0002] ITO is the abbreviation of Indium Tin Oxides. As a nanometer indium tin oxide, it has good conductivity and transparency, and can cut off harmful electron radiation, ultraviolet rays and far infrared rays that are harmful to the human body. Therefore, indium tin oxide is usually sprayed on glass, plastic and electronic display screens, used as a transparent conductive film, and at the same time reduces harmful electron radiation and ultraviolet and infrared radiation. [0003] Etching is the technique of removing material using chemical reaction or physical impact. Etching techniques are divided into wet etching and dry etching. Among them, wet etching uses chemical reagents to achieve the purpose of etching through chemical reactions. Thin-film field-effect transistor liquid crystal di...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C09K13/06
Inventor 殷福华邵勇朱龙
Owner JIANGYIN JIANGHUA MICROELECTRONICS MATERIAL
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products