Hollow glass microbead-doped porous efficient recarburizing agent recycling waste graphite electrode, and preparation method thereof

A technology of hollow glass microspheres and waste graphite, which is applied in the field of recarburizers, can solve problems such as carbon content not reaching the expected standard, poor melting effect, and affecting product performance, so as to promote graphitization process, high carbon content, The effect of improving the utilization rate

Inactive Publication Date: 2015-10-07
TONGLING MINGCHENG FOUNDRY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] During the smelting process, the carbon content in the material did not reach the expected standard due to improper ingredients, charging or excessive decarburization, which directly affected the performance of the product. Therefore, it is necessary to add a carburant during the production process. The recarburizer helps to reduce the cost of smelting production, improve the quality of smelted metals and castings, and improve the efficiency; commonly used recarburizers include artificial graphite, calcined petroleum coke, natural graphite, coke, anthracite and compounds composed of these materials However, these materials have defects such as high cost, high impurity content, poor melting effect, and low utilization rate in actual use.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0011] The carburant in this example is made of the following raw materials in parts by weight: hollow glass microspheres 1.4, nano-titanium dioxide 0.1, waste graphite electrodes 58, water glass 0.4, ammonium bicarbonate 0.1, corn stalk ash 0.3, polyethylene glycol 400 0.4, An appropriate amount of silica sol with a solid content of 10%, water 15.

[0012] Its preparation method is:

[0013] (1) Put the waste graphite electrode into 0.1mol / L dilute hydrochloric acid solution and soak for 45 minutes, then wash it with water to remove the acid, then put the electrode into 5% ethanol aqueous solution, ultrasonically clean it for 5.8 hours, and dry it completely after cleaning. Crush into particles with a particle size of ≤0.5mm, and the obtained material is used for later use;

[0014] (2) Put water glass, polyethylene glycol 400, and ammonium bicarbonate into water, stir until the materials are completely dissolved, then add corn stalk ash, stir and mix at high speed for 45 mi...

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PUM

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Abstract

The present invention relates to the field of recarburizing agents, particularly to a hollow glass microbead-doped porous efficient recarburizing agent recycling waste graphite electrode, and a preparation method thereof. According to the present invention, waste graphite electrode is adopted as a carbon material, and water glass, ammonium bicarbonate, polyethylene glycol 400 and other composite materials are used to prepare a binder; after the recarburizing agent is subjected to a high temperature firing process, the recarburizing agent has characteristics of compact and porous structure, and rapid fusion; with the added hollow glass microbeads, nanometer titanium dioxide and other ingredients, the thermal stability of the material can be improved, the impact resistance of the product can be improved, and the recarburizing process can be accelerated; silicon micro-particles are adhered on the material surface through the dried silica sol sprayed on the billet material surface so as to promote the smelting solution graphitization process and improve the material utilization rate; and the prepared recarburizing agent has characteristics of high carbon content, stable form performance, rapid and efficient recarburizing, high performance price ratio of the finished product, and effective metal product quality improving.

Description

technical field [0001] The invention relates to the field of recarburizers, in particular to a porous high-efficiency recarburizer doped with hollow glass microspheres for reusing waste graphite electrodes and a preparation method thereof. Background technique [0002] During the smelting process, the carbon content in the material did not reach the expected standard due to improper ingredients, charging or excessive decarburization, which directly affected the performance of the product. Therefore, it is necessary to add a carburant during the production process. The recarburizer helps to reduce the cost of smelting production, improve the quality of smelted metals and castings, and improve the efficiency; commonly used recarburizers include artificial graphite, calcined petroleum coke, natural graphite, coke, anthracite and compounds composed of these materials However, these materials have defects such as high cost, high impurity content, poor melting effect, and low util...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C21C7/00C22B9/10
Inventor 张蔓青肖颖
Owner TONGLING MINGCHENG FOUNDRY
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