A kind of preparation method of silk facial mask and facial mask
A mask and silk technology, which is used in skin care preparations, pharmaceutical formulations, cosmetic preparations, etc., to achieve the effects of improving water absorption, mild processing conditions, and maintaining activity.
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Embodiment 1
[0034] 1. Set the square gram weight to 15g / m 2 Soap Alkaline Scouring
[0035] Treatment solution formula:
[0036]
[0037] Note that the above solutions are prepared from water.
[0038] Process flow:
[0039] Put the gray silk into the pretreatment solution, bath ratio 1:40, soak for 30 minutes at 90°C, pH=10-10.5, remove it, wash it in hot water at 90°C for 5 minutes, take it out, and put it into the refining solution , with a bath ratio of 1:40, soak for 40 minutes at a temperature of 90°C and a pH of 10 to 10.5.
[0040] Take out the gray silk from the refining solution, soak it in hot water with a temperature of 90°C for 5 minutes, then put it into warm water with a temperature of 60°C for 5 minutes, and finally put it into the post-treatment solution and soak it at room temperature for 5 minutes, take it out, and wash it in cold water for use .
[0041] 2. Sand washing
[0042] Put the silk into a cloth bag, put it into the sand washing liquid, the bath ratio i...
Embodiment 2
[0051] 1. Set the square gram weight to 30g / m 2 soap scouring
[0052] Treatment solution formula:
[0053]
[0054] Process flow:
[0055] Pretreatment (90°C, 50min, pH=10~10.5)→hot water washing (90°C, 5min)→scouring (90°C, 40min, pH=10)→hot water washing (90°C, 5min)→warm water washing (60°C , 5min) → post-treatment solution (room temperature, 5min) → cold water washing.
[0056] 2. Sand washing
[0057] Put the silk into a cloth bag→sand washing (bath ratio 1:40, sand washing solution contains 10g / L soda ash, 0.8g / L flat plus O, 60°C, 30min)→water washing→neutralization (0.5g / L acetic acid, room temperature , 5min)
[0058] 3. Graft modification
[0059] Grafting (1:12, 1% modifier HF-M, 1h, 40°C, pH=8)→Washing
[0060] The modifier HF-M is obtained by mixing tetradecyldimethylglycidyl ammonium chloride and 3-sulfopropyldodecyldiglycidyl betaine in a mass ratio of 3:2.
[0061] 4 neutralization
[0062] 0.5g / L acetic acid, room temperature, 30min, pH=6
[0063...
Embodiment 3
[0067] 1. Change the square gram weight to: 50g / m 2 soap scouring
[0068] Treatment solution formula:
[0069]
[0070]
[0071] Process flow:
[0072] Pretreatment (90°C, 30min, pH=10~10.5)→hot water washing (80°C, 5min)→scouring (90°C, 60min, pH=10)→hot water washing (80°C, 5min)→warm water washing (40°C , 5min) → post-treatment solution (room temperature, 3min) → cold water washing
[0073] 2. Sand washing
[0074] Put the silk into a cloth bag→sand washing (bath ratio 1:40, sand washing solution contains 12g / L soda ash, 1g / L flat plus O, 60°C, 20min)→water washing→neutralization (0.5g / L acetic acid, room temperature, 5min)
[0075] 3. Graft modification
[0076] Grafting (1:20, 0.8% modifier HF-J, 2h, room temperature, pH=8) → washing with water, here, use dodecyl dimethyl epoxypropyl ammonium chloride or tetradecyl Dimethylglycidyl ammonium chloride is acceptable.
[0077] 4 neutralization
[0078] 0.5g / L acetic acid, room temperature, 30min, pH=6
[0079...
PUM
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