Method of plugging leak of medium-depth well via cross-linked polymer gel plugging agent
A technology of cross-linked polymer and plugging agent, which is applied in the field of oil drilling, can solve the problems of long plugging time, poor plugging efficiency, and short validity period, and achieve the effect of high gel strength
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Embodiment 1
[0018] A method for medium-deep well plugging using a cross-linked polymer gel plugging agent of the present invention comprises the following steps in sequence:
[0019] ⑴ Prepare raw materials with the following components and weight content, refined cotton sodium salt solution: 120 parts, acrylamide: 75 parts, ammonium persulfate: 13 parts, cerium sulfate: 2 parts, β-D-mannuronic acid (M): 4 parts, ammonium dihydrogen phosphate: 1 part, composite portland cement slurry: 100 parts and hybrid microfiber: 150 parts; the water-cement ratio of the composite portland cement slurry is 0.44;
[0020] (2) Add acrylamide to the refined cotton sodium salt solution, stir at a high speed of 400r / min for 10 minutes to fully mix the two, then stir at a medium speed at a speed of 300r / min, heat to 60°C while stirring at a medium speed maintain a constant temperature;
[0021] (3) Continuously feed nitrogen gas into the reaction product of step (2) and the reaction vessel. After feeding ni...
Embodiment 2
[0032] A method for medium-deep well plugging using a cross-linked polymer gel plugging agent of the present invention comprises the following steps in sequence:
[0033] ⑴ Prepare raw materials with the following components and weight content, refined cotton sodium salt solution: 120 parts, acrylamide: 80 parts, ammonium persulfate: 15 parts, cerium sulfate: 3 parts, β-D-mannuronic acid (M): 4 parts, ammonium dihydrogen phosphate: 1.2 parts, composite Portland cement slurry: 100 parts and hybrid microfiber: 180 parts; the water-cement ratio of the composite Portland cement slurry is 0.44;
[0034] (2) Add acrylamide to the refined cotton sodium salt solution, stir at a high speed of 400r / min for 10 minutes to fully mix the two, then stir at a medium speed at a speed of 300r / min, heat to 60°C while stirring at a medium speed maintain a constant temperature;
[0035] (3) Continuously feed nitrogen gas into the reaction product of step (2) and the reaction vessel. After feeding...
Embodiment 3
[0046] A method for medium-deep well plugging using a cross-linked polymer gel plugging agent of the present invention comprises the following steps in sequence:
[0047] ⑴ Prepare raw materials for the following components and weight content, refined cotton sodium salt solution: 120 parts, acrylamide: 85 parts, ammonium persulfate: 17 parts, cerium sulfate: 5 parts, β-D-mannuronic acid (M): 4 parts, ammonium dihydrogen phosphate: 1.5 parts, composite Portland cement slurry: 100 parts and hybrid microfiber: 200 parts; the water-cement ratio of the composite Portland cement slurry is 0.44;
[0048] (2) Add acrylamide to the refined cotton sodium salt solution, stir at a high speed of 400r / min for 10 minutes to fully mix the two, then stir at a medium speed at a speed of 300r / min, heat to 60°C while stirring at a medium speed maintain a constant temperature;
[0049] (3) Continuously feed nitrogen gas into the reaction product of step (2) and the reaction vessel. After feeding ...
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