Antifouling system comprising silicone hydrogel
A system, anti-fouling technology, applied in biocide-containing paints, anti-fouling/underwater coatings, adhesives, etc., can solve the problem of low efficiency of amino silicone resin
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Embodiment 1
[0160] Example 1. Synthesis of SiPEG
[0161] Will 217g have the nominal structure H MD 10 m H Hydride-terminated α,ω-(SiH)polydimethylsiloxane, 36.8g vinyltrimethoxysilane, 420g toluene and 0.13g chlorotris(triphenylphosphine)rhodium(I) were added to the equipment have N 2 Inlet, condenser and thermometer in a three-neck round bottom flask. put the solution in N 2 Mix under atmosphere for 30 minutes, then heat to 80° C. for 12 hours to give a light yellow solution.
[0162] Add 120 g of the solution to a 2 Inlet, condenser and thermometer in another three-neck round bottom flask. The reaction flask was further charged with 20.8 g of polyethylene glycol monoallyl ether (8 oxirane groups), 24 g of toluene and 0.125 g of Karstedt's catalyst in isopropanol (1% of Pt). put the solution in N 2 Mix for 30 minutes, then heat to 100°C for 2 hours. The resulting solution contained 40% SiPEG with the following chemical structure:
[0163]
Embodiment 2
[0164] Example 2. Synthesis of Hybrid Adhesion Promoters.
[0165] Before use, 10.14 g of Epilote 828 (from Momentive Specialty Chemicals), 42 g of toluene, and 32 g of SF1706 from Momentive Performance Materials (dimethoxysilyl-terminated and amine-grafted curable aminosilicone) were added to a beaker and cooled at ambient Mix for 4 hours.
Embodiment 3
[0166] Example 3. Preparation of epoxy coating
[0167] Epoxide-containing Epon 828 (from Momentive Specialty Chemicals) mixed with amine (Epikure 3292-FX-60 from Momentive Specialty Chemicals), and in some cases the adhesion promoter of Example 2, was cured under ambient conditions. According to the formula of Table 1, feed intake is added in the plastic container.
[0168] Table 1
[0169]
[0170] Epon 828
[0171] Mixing was done using SpeedMixerDAC150 from FlackTech company. Once the coating was cured, when the mixed adhesion promoter was included in Example 3B, the water contact angle increased from 70° for the standard epoxy (Example 3A) to 92°, indicating the presence of silicone moieties on the coating surface.
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