Method for preparing high polymer material cold accumulation agent
A technology of polymer materials and cold storage agents, which is applied in heat exchange materials, chemical instruments and methods, etc., can solve the problems of short cold storage time, narrow phase transition temperature range, large latent heat of freeze-thaw phase transition, etc. The effect of long duration, large latent heat of freeze-thaw phase transition, and long cold storage time
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Embodiment 1
[0032] A method for preparing a polymer material cool storage agent, comprising the following specific process steps:
[0033] 1) Make a 0.32~0.89% aqueous solution of polymers containing hydrophilic groups in the molecular structure;
[0034] 2) Acrylic acid with a neutralization degree of 62.5~73.2% and a mass fraction of 0.73~0.86, and hydroxyethyl methacrylate with a neutralization degree of 65~72.5% and a mass fraction of 0.21~0.32, and a neutralization degree of 66.5~ 74% and three monomers of maleic anhydride with a mass fraction of 0-0.08 are added to the aqueous solution of step 1), and mixed evenly to make a mixed solution;
[0035] 3) Add acrylic acid, hydroxyethyl methacrylate and maleic anhydride to the mixed solution in step 2), and add ethylene glycol diacrylate crosslinking agent with a total mass of 0.08-0.23% of the three monomers, stir and dissolve;
[0036] 4) Add potassium persulfate initiator of 0.05-0.45% of the total mass of the three monomers of acryl...
Embodiment 2
[0039] This embodiment is further optimized on the basis of the above-mentioned embodiments. In order to further realize the present invention, the following steps are specially provided: the polymer is carboxymethyl cellulose, hydroxyethyl cellulose, seaweed Sodium acrylate, carboxymethyl starch, hydroxypropyl starch or sodium polyacrylate.
Embodiment 3
[0041] This embodiment is further optimized on the basis of any of the above-mentioned embodiments. In order to further realize the present invention, the following steps are specially provided: the drying time in the step 4) is 2 to 4 hours, and the pulverization to 60~90 mesh.
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