Thick film circuit insulating dielectric slurry for aluminum substrates, and preparation method thereof
A thick-film circuit and insulating medium technology, which is applied in the field of high-power metal aluminum substrate thick-film circuit insulating medium slurry and its preparation, can solve the problems of inability to use high-temperature sintering process, slow heating rate of stainless steel substrate, and large thermal expansion coefficient of metal aluminum, etc. Problems, to achieve the effect of large-scale industrial production, good insulation performance, high breakdown voltage
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Embodiment 1
[0017] Accurately weigh 32gBa 3 (PO 4 ) 2 , 11gAlPO 4 , 5gZn 3 (PO 4 ) 2 , 4gSn 2 P 2 o 7 , 26gRb 2 O, 20gB 2 o 3 , 2gNb 2 o 5 .
[0018] The organic liquid carrier components are terpineol, tributyl citrate, ethyl cellulose, Span 85, 1,4-butyrolactone, hydrogenated castor oil, the mass ratio is 73:12:4:6:4:1 .
[0019] Mix the raw materials evenly according to the proportion, place them in a high-temperature electric furnace, heat them up to 1350°C at a heating rate of 5°C / min, keep them warm for 3 hours, then perform water quenching, put the solids into the corundum tank of the planetary ball mill, and then add deionized Water is used as the mixing medium and ball milled for 4 hours to obtain a composite glass-ceramic powder with a particle size of 1-4 μm; the composite glass-ceramic powder and the organic liquid carrier are made into a slurry at a mass ratio of 75:25, and the three-roll rolling mill is used repeatedly rolling.
[0020] The film is printed o...
Embodiment 2
[0022] Accurately weigh 25gBa 3 (PO 4 ) 2 , 15gAlPO 4 , 4gZn 3 (PO 4 ) 2 , 8gSn 2 P 2 o 7 , 30gRb 2 O, 15gB 2 o 3 , 3gNb 2 o 5 .
[0023] The organic liquid carrier components are terpineol, tributyl citrate, ethyl cellulose, Span 85, 1,4-butyrolactone, hydrogenated castor oil, the mass ratio is 75:10:5:5:3:2 .
[0024] Mix the raw materials evenly according to the proportion, place them in a high-temperature electric furnace, heat them up to 1400°C at a heating rate of 8°C / min, keep them warm for 2 hours, then perform water quenching, put the solids into the corundum tank of the planetary ball mill, and then add deionized Water is used as the mixing medium and ball milled for 3 hours to obtain a composite glass-ceramic powder with a particle size of 2-5 μm; the composite glass-ceramic powder and the organic liquid carrier are made into a slurry at a mass ratio of 78:22, and the three-roll rolling mill is used repeatedly rolling.
[0025] The film is printed o...
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