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Preparation method of coffee ground activated carbon

A technology for activated carbon with grounds and coffee grounds, which is applied in the field of preparation of activated carbon with coffee grounds, can solve the problems of clogging the activated carbon with coffee grounds, the ineffectiveness of coffee grounds, and the reduction of the activation effect of medicines, etc., and achieves a simple and feasible carbon-making process, low price, and working conditions. The effect of parameter stabilization

Inactive Publication Date: 2016-01-06
GUANGDONG UNIV OF TECH
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Problems solved by technology

[0003] With the development of human society and the increasing awareness of environmental protection, activated carbon is widely used in industrial purification, environmental pollution prevention and other fields. However, the lack of resources makes people choose activated carbon from factors such as activation difficulty, raw material grade, price, and supply. The raw materials have changed from the previous woody raw materials to coal, petroleum, etc., and then to relatively cheap plant straw, coconut shell, date shell, bagasse, pulp waste liquid, etc., but there is little research on the preparation of activated carbon from coffee grounds.
[0004] Activated carbon from coffee grounds can be used as an air purification material to absorb odors in the air. At present, the drug activation method has the advantages of simultaneous carbonization and activation and is widely used, but this method is not effective for coffee grounds because coffee grounds contain a lot of Grease, these greases will block the pores of the coffee grounds activated carbon and reduce the activation effect of the drug. Therefore, how to remove the grease from the coffee grounds and prepare high-performance activated carbon is the key to the current technology

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Embodiment Construction

[0029] Below in conjunction with specific embodiment the present invention is described in further detail:

[0030] Table 1 lists the activation temperature, vacuum degree, activation time, impregnation ratio, and heating rate of several examples of the present invention, among which Example 17 to Example 21 are comparative examples.

[0031] First, wash the coffee grounds from an instant coffee factory in Dongguan City, Guangdong Province with distilled water to remove impurities (ash and water-soluble substances), and dry the washed coffee grounds in a 50°C oven for 48 hours; then take the dried coffee Put the slag into the quartz boat and place it in the tubular resistance furnace, then connect the condensation system and the non-condensable gas absorption system, start the vacuum pump after checking that there is no air leakage in the system, and adjust the pressure control valve to maintain the pyrolysis vacuum degree in Table 1 Under the numerical value, adjust the param...

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Abstract

The invention discloses a preparation method of coffee ground activated carbon. The preparation method comprises the steps of pretreatment, degreasing, dipping, activization, washing and the like. Firstly, vacuum pyrolysis degreasing is performed on coffee grounds to remove grease in the coffee grounds and carbonization is performed to obtain a precursor of the coffee grounds; then phosphoric acid is taken as an activating agent for dipping and ultrasound at different dipping ratios (the mass ratio of the phosphoric acid with the precursor of the coffee grounds); activating under different vacuum conditions after drying; the effect of the activation conditions of activation final temperature, vacuum degree, heating rate, activation time, the dipping ratio and the like on the performance of the coffee ground activated carbon is overall considered, the prepared coffee ground activated carbon is high in yield, and the iodine adsorption value and methylene blue adsorption value are both above the state first level activated carbon standard (the iodine adsorption value is 1000mg / g and the methylene blue adsorption value is 135mg / g); the coffee ground activated carbon can be used for adsorbing hazardous gas such as formaldehyde in a room after decoration, and is an air purification material with a very good adsorptive property; the whole carbon preparation process has the advantages that the blockage of coffee ground activated carbon pores caused by the coffee ground grease is avoided, the working state parameters are stable, green and environmental protection and non-pollution are realized, and is simple and feasible.

Description

technical field [0001] The invention relates to the technical field of recycling waste materials, in particular to a method for preparing activated carbon from coffee grounds. Background technique [0002] As the first of the three major beverages in the world, coffee is the second largest trade product after oil, and plays a pivotal role in daily life and commercial trade. According to the statistics of relevant departments, at the end of the "Eleventh Five-Year Plan", the total area of ​​coffee planting in my country will grow to more than 600,000 mu. From a global perspective, by 2014, the output of coffee was 7.3159 million tons per year. However, every 1 kg of instant coffee produced will produce 0.9 kg of coffee grounds. How to recycle coffee grounds has become a new topic in recent years. [0003] With the development of human society and the increasing awareness of environmental protection, activated carbon is widely used in industrial purification, environmental po...

Claims

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Application Information

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IPC IPC(8): C01B31/12
Inventor 孙水裕任杰陈楠伟林伟雄叶茂友
Owner GUANGDONG UNIV OF TECH
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