Vertical type tubulation heat exchange extraction tank and application thereof
A vertical tube and heat extraction technology, applied in the direction of solid solvent extraction, etc., can solve the problems of difficult discharge, cross contamination, uneven temperature in the extraction process, etc., and achieve the effect of reducing heat loss
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Embodiment 1
[0118] figure 1 It is a schematic cross-sectional structure diagram of the present invention; figure 2 It is a schematic diagram of the top view structure.
[0119] Such as figure 1 A vertical tube-and-tube heat exchange extraction tank is shown, which is characterized in that it includes a condenser assembly, a stirring assembly, a tank body, a CIP device, a self-circulation device, and a rotary filter device.
[0120] Such as figure 1 The illustrated condenser assembly 17 includes a condenser 18 , a cooler 19 , a juice gas line 20 , a U-shaped return line 15 and a sampling port 21 . The condenser 18 is located at the top of the condenser assembly 17, and is connected to the upper head 41 of the tank 1 through the juice pipe 20, the cooler 19 is located below the condenser 18, and the U-shaped return pipe 15 is located below the cooler 19 and passes through the valve It is connected with the upper head 41 of the tank body 1 .
[0121] Such as figure 1The stirring assem...
Embodiment 2
[0127] Such as figure 1 The condenser assembly shown is used to condense the rising solvent during the extraction process and is a reflux extraction unit. The condenser assembly includes a juice vapor pipe, a condenser, a cooler, a U-shaped return pipe, and a sampling port.
[0128] Such as figure 1 The stirring assembly shown is on the central axis of the tank body and mainly plays a mixing role during the extraction process. Including motor, motor reducer, reducer base, mechanical seal, stirring shaft, stirring blade.
[0129] Such as figure 1 , figure 2 As shown: the vertical tube heat exchange tank is the main part of the equipment, including three parts: the upper head, the main body and the lower head. The tank body is cylindrical, and the lower head is inverted cone. Mechanical seal, elliptical pressure hand hole, CIP port A, CIP port B, solvent inlet, return port, explosion-proof sight lamp, vacuum gauge port, thermometer port, vacuum port, breathing port and cir...
Embodiment 3
[0134] The extraction method of scorpion peptide is carried out by using a vertical tube heat exchange scorpion peptide extraction tank:
[0135] (1) Throwing the scorpion: After crushing, the scorpion is thrown into the tank through vacuum suction or oval pressure hand hole;
[0136] (2) Add organic solvent: inject a certain amount of organic solvent into the tank through nitrogen pressure or vacuum;
[0137] (3) Mixing: Turn on the stirring and self-circulation device to mix the material and organic solvent evenly;
[0138] (4) Extraction: Open the industrial steam valve, the industrial steam enters the jacket through the inlet of the heating and cooling medium, and the condensed water is discharged through the outlet of the heating and cooling medium, and at the same time, the material in the tank is heated, and the heat preservation time is kept; during the heat preservation process, the condenser assembly is turned on The low-temperature cooling water is used to condense...
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