Photosensitive resin composition for forming insulating film in organic el display element
A technology of photosensitive composition and photosensitive resin, which is applied in the direction of photosensitive materials used in opto-mechanical equipment, etc., can solve the problems of easy cracking and poor display of the functional layer, and achieve the effect of high water resistance
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[0160] □Preparation method of photosensitive resin composition□
[0161] The photosensitive resin composition can be prepared by mixing and stirring the above-mentioned components in a predetermined ratio, and then by a normal method. In addition, filtration may be further performed using a net, a membrane filter, or the like as necessary.
[0162] □How to form an insulating film□
[0163] The insulating film is formed by a method comprising: a coating step of forming a coating film of the photosensitive resin composition on a substrate; an exposure step of positionally selectively irradiating the coating film with active rays to expose; The development process of developing the coated film.
[0164] [Coating process]
[0165] In the coating step, the photosensitive resin composition is coated on a substrate for forming an EL display element having various functional layers as necessary, using a spin coater or the like to form a coating film. The film thickness of the coat...
Embodiment 1~11、 and comparative example 1~9
[0174] (resin component)
[0175] In Examples and Comparative Examples, the resins described in Table 1 below were used as the resin component (A) novolac resin or a substitute component of (A) novolac resin.
[0176] Among the resin components described in Table 1 below, as the cresol novolac resin, a resin prepared according to the following formulation was used.
[0177]
[0178] m-cresol and p-cresol, formaldehyde, and catalytic amount of oxalic acid in the ratios described in Table 1 were put into the reaction vessel. The contents of the reaction vessel were reacted under reflux conditions for 4 hours according to a conventional method to prepare a crude cresol novolak resin. Thereafter, the crude cresol novolak resin was heated under reduced pressure to remove low molecular weight components in the resin to obtain a cresol novolac resin. By adjusting the heating temperature and treatment time in the heating step under reduced pressure, the contents of monomers and di...
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