Straw fiber-based biomass composite material and preparation method thereof
A composite material and straw fiber technology, applied in the field of straw-based biomass composite materials and their preparation, can solve the problems of shortage of fiber sources, large specific gravity, low strength, etc., and achieve high social and economic benefits.
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Embodiment 1
[0012] (1) Take 100 parts (mass parts) of straw with a moisture content of 5% or less and a length of 20 mm or less, 10 parts of 60% acetic acid aqueous solution, 2 parts of diesel oil, blend them evenly, and put them in a sealed vacuum furnace , at a vacuum degree of less than or equal to 50Pa, at a temperature of 200°C, sinter for 15 minutes, then take out and pulverize, sieve to control the particle size at 10 mesh, and set aside
[0013] (2) Take 60 parts of fiber obtained in step (1), 40 parts of HDPE, 1 part of titanate coupling agent, 1 part of aluminate coupling agent, 2 parts of polyethylene glycol, 5 parts of EAA, 1 part of polyethylene wax, 0.5 parts of maleic anhydride, blended in a high-speed mixer for 10 minutes, and set aside.
[0014] (3) Extrude and granulate the mixed materials through a screw extruder, controlling the head temperature to 190°C, head pressure to 3MPa, and screw speed to 80r / min.
[0015] Table 1
[0016]
Embodiment 2
[0018] (1) Take 100 parts (mass parts) of straw with a moisture content of 5% or less and a length of 20 mm or less, 15 parts of acetic acid aqueous solution with a concentration of 65%, and 4 parts of diesel oil, and blend them evenly and put them in a sealed vacuum furnace , at a vacuum degree of less than or equal to 50Pa, at a temperature of 250°C, sinter for 20 minutes, then take out and pulverize, sieve to control the particle size at 20 mesh, and set aside
[0019] (2) Take 70 parts of fiber obtained in step (1), 30 parts of HDPE, 2 parts of titanate coupling agent, 2 parts of aluminate coupling agent, 3 parts of polyethylene glycol, 7 parts of EAA, 2 parts of polyethylene wax, 1 part of maleic anhydride, blended in a high mixer for 20 minutes, set aside.
[0020] (3) Extrude and granulate the mixed materials through a screw extruder, controlling the head temperature to 190°C, head pressure to 3MPa, and screw speed to 80r / min.
[0021] Table 2
[0022]
Embodiment 3
[0024] (1) Take 100 parts (mass parts) of straw with a moisture content of 5% or less and a length of 20 mm or less, 20 parts of 70% acetic acid aqueous solution, and 5 parts of diesel oil, mix them evenly and put them in a sealed vacuum furnace , at a vacuum degree of less than or equal to 50Pa, at a temperature of 300°C, sinter for 30 minutes, then take out and pulverize, sieve to control the particle size at 30 mesh, and set aside
[0025] (2) Take 80 parts of fiber obtained in step (1), 40 parts of HDPE, 3 parts of titanate coupling agent, 3 parts of aluminate coupling agent, 4 parts of polyethylene glycol, 10 parts of EAA, 3 parts of polyethylene wax, 1.5 parts of maleic anhydride, blended in a high mixer for 30 minutes, set aside.
[0026] (3) Extrude and granulate the mixed materials through a screw extruder, controlling the head temperature to 190°C, head pressure to 3MPa, and screw speed to 80r / min.
[0027] table 3
[0028]
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