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Preparation method of ultrasonically dispersed zirconium boride boron carbide-carbon fiber friction material

A technology of zirconium boride, boron carbide and friction materials, which is applied in the field of preparation of friction materials, can solve problems such as potential safety hazards and reduced friction performance, and achieve the effects of improving wear resistance, high friction performance and high manufacturing cost

Inactive Publication Date: 2018-06-08
SHANDONG UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In addition, the friction performance of C / C composite materials will be reduced in a humid environment, which will bring serious safety hazards to the use.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] (1) Set the density to 1.8g / cm 3 The graphitized carbon fiber blanket is fed with a mixed gas of propane gas and nitrogen at a temperature of 900°C. The molar ratio of propane gas: nitrogen is 1:4, the flow rate is controlled at 50ml / min, and the carburizing treatment is performed for 24 hours to obtain a carburized carbon fiber blanket. ;

[0020] (2) Pass the above-mentioned carburized carbon fiber blanket into a mixed gas of boron trichloride, methane, hydrogen and argon at a temperature of 900 °C, and the molar ratio of boron trichloride: methane: hydrogen: argon is 1:1: 3:4, the flow rate is controlled at 50ml / min, and the deposited boron carbide is treated for 24 hours to obtain a deposited boron carbide carbon fiber blanket;

[0021] (3) Immerse the above-mentioned deposited boron carbide carbon fiber blanket into a slurry with a particle size of less than 0.3 μm and a content of 5% zirconium boride, place it in an ultrasonic cleaner and fill it with zirconium b...

Embodiment 2

[0025] (1) Set the density to 0.8g / cm 3 The graphitized carbon fiber blanket is fed with a mixture of propane gas and nitrogen at a temperature of 1000°C. The molar ratio of propane gas: nitrogen is 1:5, the flow rate is controlled at 350ml / min, and the carburizing treatment is performed for 18 hours to obtain a carburized carbon fiber blanket. ;

[0026] (2) Pass the above-mentioned carburized carbon fiber blanket into a mixed gas of boron trichloride, methane, hydrogen and argon at a temperature of 1000 °C, and the molar ratio of boron trichloride: methane: hydrogen: argon is 1:1.5: 4.5:5, flow control at 350 ml / min, deposited boron carbide treatment for 17 hours to obtain deposited boron carbide carbon fiber blanket;

[0027] (3) Immerse the above-mentioned deposited boron carbide carbon fiber blanket into a slurry with a particle size of less than 0.3 μm and a content of 12% zirconium boride, place it in an ultrasonic cleaner and fill it with zirconium boride for 40 minut...

Embodiment 3

[0031] (1) Set the density to 0.1g / cm 3 The graphitized carbon fiber blanket is passed into a mixed gas of propane gas and nitrogen at a temperature of 1100 ° C. The molar ratio of propane gas: nitrogen is 1: 6, the flow rate is controlled at 600ml / min, and the carburizing treatment is performed for 10 hours to obtain a carburized carbon fiber blanket. ;

[0032] (2) Pass the above-mentioned carburized carbon fiber blanket into a mixed gas of boron trichloride, methane, hydrogen and argon at a temperature of 1100 °C, and the molar ratio of boron trichloride: methane: hydrogen: argon is 1:2: 6:6, the flow rate is controlled at 600ml / min, and the deposited boron carbide is treated for 10 hours to obtain a deposited boron carbide carbon fiber blanket;

[0033] (3) Immerse the above-mentioned deposited boron carbide carbon fiber blanket into a slurry with a particle size of less than 0.3 μm and a content of 20% zirconium boride, place it in an ultrasonic cleaner and fill it with ...

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Abstract

A method for preparing an ultrasonic dispersion zirconium diboride boron carbide-carbon fiber friction material is characterized in that a graphitized carbon fiber blanket with the density being 0.1-1.8 g / cm<3> is subjected to carburizing treatment, then subjected to boron carbide deposition, subjected to ultrasonic dispersion zirconium diboride filling treatment and subjected to embedding siliconizing, and then nitridation is carried out in the nitrogen atmosphere to prepare the ultrasonic dispersion zirconium diboride boron carbide-carbon fiber friction material. According to the method, the graphitized carbon fiber blanket is adopted, and the friction material is prepared through the steps of carburization, silicon carbide deposition, zirconium diboride filling, embedding siliconizing, nitridation and the like. The prepared friction material is high in strength, toughness and friction performance and can adapt to various climatic conditions.

Description

technical field [0001] The invention relates to a preparation method of a friction material composited by carbon fiber and ceramic material, and belongs to the technical field of composite material preparation. Background technique [0002] At present, carbon fiber and carbon (C / C) composite materials are mainly used as friction materials. Since the wear resistance of C / C composite materials is relatively low, people are looking for a method for preparing friction materials with higher wear resistance. In addition, the friction performance of C / C composite materials will be reduced in a humid environment, which will bring serious safety hazards to the use. Contents of the invention [0003] The object of the present invention is to provide a method for preparing a friction material that can overcome the above-mentioned defects, achieve higher strength, higher friction performance and adapt to various climatic conditions. Its technical solution is: [0004] The method of ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B38/00C04B35/80C04B35/563C04B35/58C04B35/573C04B35/591C04B35/65C04B35/622C04B35/632
CPCC04B35/563C04B35/573C04B35/58078C04B35/591C04B35/622C04B35/632C04B38/00C04B2111/40C04B2111/00362C04B2235/5248C04B2235/5256C04B2235/46C04B2235/616C04B2235/6567C04B2235/658
Inventor 唐竹兴
Owner SHANDONG UNIV OF TECH
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