Composite type ultrahigh water filling material and preparation method thereof
A filling material and ultra-high water technology, applied in the field of materials, can solve the problems of long setting and hardening time, affecting the conveying effect, complicated construction technology, etc., and achieve perfect structure and performance, simple and easy preparation method, and good fluidity of slurry Effect
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Embodiment 1
[0023] A composite ultra-high water filling material, formula: the filling material is composed of A slurry and B slurry with a volume ratio of 1:1, A slurry is composed of 1000gA1, 100gA2 and 4000g water, B slurry is composed of 1000gB1, 100gB2 and 4000g of water;
[0024] The parts by weight of A1 consist of: 85 parts of sulphoaluminate cement clinker, 7 parts of fly ash, and 8 parts of composite additive;
[0025] The parts by weight of A2 consist of: 100 parts of polyoxypropylene glycol, 1 part of triethylenetetramine;
[0026] The composition of composite additive 1 in parts by weight is: 10 parts of sodium chloride, 20 parts of sodium sulfate, 60 parts of sodium metaaluminate, 5 parts of sodium gluconate, and 5 parts of hydroxypropyl methylcellulose;
[0027] The parts by weight of B1 consist of: 70 parts of gypsum, 20 parts of lime, 7 parts of fly ash, 3 parts of composite additive two;
[0028] The parts by weight of B2 consist of: 85 parts of diphenylmethane diisocy...
Embodiment 2
[0041] A composite ultra-high water filling material, formula: composite admixture 1, composite admixture 2, A1, A2, B1, and B2 are the same as in Example 1, except that the A slurry is composed of 1000gA1, 150gA2 and 6000g of water. The B slurry consisted of 1000g B1, 150g B2 and 6000g water.
[0042] Preparation method: the steps are the same as in Example 1, and the only difference from Example 1 is that the amount of each raw material is weighed according to the formula of the filling material in Example 2.
[0043] It is tested by sampling: the single-liquid storage time of A slurry and B slurry is 28 hours and 32 hours respectively, the single-liquid fluidity of A slurry and B slurry is 325mm and 335mm respectively; the hardening time of the mixed slurry is 61min, 2h compressive strength is 0.26MPa, 28d compressive strength is 1.22MPa, and the seed setting rate is 98.3%.
Embodiment 1-2
[0045] 1. The single liquid storage time, the hardening time of the mixed slurry and the compressive strength refer to the 6.4 single slurry setting time and 6.3 gelling time in the coal industry standard of the People's Republic of China "High Water Filling Materials" (MT / T420-1995) , 6.2 compressive strength;
[0046] 2. Refer to GB50119-2003 Appendix A for fluidity of single liquid;
[0047] 3. The setting rate refers to the solid volume Vs after the slurry solidifies and the initial volume V of the slurry 0 ratio, expressed as a percentage. If the seed setting rate is greater than 1, the fruit body expands; if the seed setting rate is less than 1, the fruit body shrinks.
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