A composite ultra-high water filling material and its preparation method
A filling material, ultra-high water technology, applied in the field of materials, can solve the problems of long condensation and hardening time, complicated construction process, affecting the conveying effect, etc., to achieve perfect structure and performance, good slurry fluidity, and simple and feasible preparation method. Effect
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Embodiment 1
[0023] A composite ultra-high water filling material, formula: the filling material is composed of A slurry and B slurry with a volume ratio of 1:1, A slurry is composed of 1000g A1, 100g A2 and 4000g water, and B slurry is composed of 1000g B1, 100g B2 and 4000g water;
[0024] The parts by weight of A1 consist of: 85 parts of sulphoaluminate cement clinker, 7 parts of fly ash, and 8 parts of composite additive;
[0025] The parts by weight of A2 consist of: 100 parts of polyoxypropylene glycol, 1 part of triethylenetetramine;
[0026] The composition of composite additive 1 in parts by weight is: 10 parts of sodium chloride, 20 parts of sodium sulfate, 60 parts of sodium metaaluminate, 5 parts of sodium gluconate, and 5 parts of hydroxypropyl methylcellulose;
[0027] The parts by weight of B1 consist of: 70 parts of gypsum, 20 parts of lime, 7 parts of fly ash, 3 parts of composite additive two;
[0028] The parts by weight of B2 consist of: 85 parts of diphenylmethane di...
Embodiment 2
[0041] A composite ultra-high water filling material, formula: composite admixture 1, composite admixture 2, A1, A2, B1, and B2 are the same as in Example 1, except that the A slurry is composed of 1000g A1, 150g A2 and 6000g water Composition, B slurry consisted of 1000g B1, 150g B2 and 6000g water.
[0042] Preparation method: the steps are the same as in Example 1, and the only difference from Example 1 is that the amount of each raw material is weighed according to the formula of the filling material in Example 2.
[0043] It is tested by sampling: the single liquid storage time of A slurry and B slurry is 28 hours and 32 hours respectively, the single liquid fluidity of A slurry and B slurry is 325mm and 335mm respectively; the hardening time of mixed slurry is 61min, 2h compressive strength is 0.26MPa, 28d compressive strength is 1.22MPa, and the seed setting rate is 98.3%.
Embodiment 1-2
[0045] 1. The storage time of the single liquid, the hardening time of the mixed slurry and the compressive strength refer to 6.4 single slurry setting time and 6.3 gelling in the coal industry standard of the People's Republic of China "High Water Filling Materials" (MT / T 420-1995) Time, 6.2 compressive strength;
[0046] 2. The fluidity of single liquid is carried out according to Appendix A of GB 50119-2003;
[0047] 3. The setting rate refers to the solid volume Vs after the slurry solidifies and the initial volume V of the slurry 0 ratio, expressed as a percentage. If the seed setting rate is greater than 1, the fruit body expands; if the seed setting rate is less than 1, the fruit body shrinks.
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