Method for preparing tert-butyl hydroperoxide
A technology of tert-butyl hydroperoxide and di-tert-butyl peroxide, applied in the field of preparation of tert-butyl hydroperoxide, can solve problems such as unfavorable environmental protection, a large amount of waste sulfuric acid, etc., and achieves less reaction by-products and low degree of corrosion , the effect of high product purity
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Embodiment 1
[0013] Embodiment 1, a kind of preparation method of tert-butyl hydroperoxide, raw materials used are isobutane and di-tert-butyl peroxide, according to a certain ratio, form at high temperature and high pressure, through catalysis, vacuum distillation, crystallization; The mass ratio of the raw material isobutane to di-tert-butyl peroxide is 1:1-3; the high temperature and high pressure conditions are 140-160°C and 1.5-2.5 atmospheres; the catalyst is iron potassium oxalate; The vacuum distillation conditions are 0.1-0.3 atmospheric pressure and the temperature is 30-40°C; the crystallization is to dissolve the collected liquid with distilled water at 20-40°C, then cool down to 1-5°C, stir gently, and statically Set crystallization.
Embodiment 2
[0014] Embodiment 2, in the preparation method of a kind of tert-butyl hydroperoxide described in embodiment 1: the mass ratio of described raw material isobutane and di-tert-butyl peroxide is 1:2.
Embodiment 3
[0015] Embodiment 3, in the preparation method of a kind of t-butyl hydroperoxide described in embodiment 1: described high temperature, high pressure condition is 150 ℃, 2.5 atmospheric pressure.
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