Efficient shrinkage-reducing anti-cracking agent and preparation method thereof
A technology of anti-cracking agent and shrinkage reducing agent, which is applied in the field of high-efficiency shrinkage-reducing anti-cracking agent and its preparation, which can solve the problems of concrete strength loss, high cost, and less active ingredients, so as to improve the effectiveness of expansion, expand the scope of use, and delay the early stage. The effect of hydration
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[0017] 1. Preparation of shrinkage reduction components
[0018] Mix 2 parts of polyethylene glycol monoallyl ether, 2 parts of methoxypolyethylene glycol methacrylate and 1 part of styrene into the reaction kettle, and mix polyethylene glycol monoallyl ether with The molar ratio of hydrogen peroxide is 5:1. Add 0.1 mol / L hydrogen peroxide solution in proportioning ingredients, raise the temperature of the reactor to 65°C, and then add 0.5 parts of polyacrylamide and 0.1 parts of ammonium persulfate initiator dropwise to the reaction at the same time. In the kettle, add dropwise separately, and the dropping time is 60min. After the dropwise addition, keep the temperature for 3 hours. After the reaction, add alkali to neutralize to pH=7.1, and obtain a light milky white transparent liquid with a solid content of 46.3%, and a molecular weight of 49000. Liquid shrinkage reducing component A with a macromonomer conversion of 91.2%.
[0019] 2. Preparation of powder high-efficienc...
Embodiment 1
[0021] Get 65 parts of f-CaO content and be 65%, particle size is the commercially available calcium oxide expansion agent of 900 meshes and joins in the powder feeder of spray-drying tower as expansion component, feeds the gas that pressure is 0.5MPa to expand component It is delivered to the front end of the hot air distributor at the top of the drying tower, and hot air with a temperature of 190°C is introduced to quickly dry the expansion component and evenly disperse it in the hot air flow. Open the spray drying tower, and when the temperature of the feed inlet at the top of the spray drying tower is 120°C, use a screw pump to transport 35 parts of the above-mentioned liquid shrinkage reduction components to the liquid feed inlet at the top of the spray drying tower, and pass through the liquid feed inlet The high-speed centrifugal atomizing disc atomizes the liquid shrinkage component into micro-droplets with a droplet diameter of 50-100 microns, and at the same time, the...
Embodiment 2
[0023] Get 60 parts of f-CaO content and be 65%, particle size is the commercially available calcium oxide expansion agent of 900 meshes and joins in the powder feeder of spray-drying tower as expansion component, feeds the gas that pressure is 0.4MPa to expand component It is delivered to the front end of the hot air distributor at the top of the drying tower, and hot air with a temperature of 180°C is introduced to quickly dry the expansion component and evenly disperse it in the hot air flow. Open the spray drying tower, and when the temperature of the feed inlet at the top of the spray drying tower is 125°C, use a screw pump to transport 40 parts of the above-mentioned liquid shrinkage reduction components to the liquid feed inlet at the top of the spray drying tower, and pass through the liquid feed inlet The high-speed centrifugal atomizing disc atomizes the liquid shrinkage component into micro-droplets with a droplet diameter of 50-100 microns, and at the same time, the...
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