A kind of long-acting antifogging agent for automobile glass and preparation method thereof
An automotive glass and anti-fogging agent technology, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of flammability, short anti-fog time, high risk, etc., to achieve enhanced durability and enhanced anti-fog effect. Effect
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[0029] The preparation method of modified nano silica sol comprises the steps:
[0030] (1), weigh each raw material in proportion, then in a 250ml there-necked bottle with a thermometer and a stirrer, add powdered nano-silicon dioxide and absolute ethanol, and stir for 10 minutes at 40°C, Then add vinyltriethoxysiloxane and stir again for 30 minutes;
[0031] (2), then add maleic anhydride, acrylic acid, methacrylic acid, and hydroxyethyl acrylate to the there-necked flask in turn, and after stirring for 10 minutes, add dibenzoyl peroxide and heat up to boiling;
[0032] (3) Boiling and reacting for 3 hours, keeping warm for 30 minutes, then adding polyvinyl alcohol and sorbitol, and stirring until completely dissolved. That is, the modified nano-silica sol is prepared.
[0033] The modified polyacrylate solutions in the following examples are all 8% solutions formed by copolymerization of acrylic acid-maleic anhydride-methacrylic acid. The preparation method of the modifi...
Embodiment 1
[0035] Described automobile glass antifogging agent, it comprises the raw material of following mass percentage composition:
[0036]
[0037]
[0038] Modified nano-silica sol (20% liquid) means that the mass percentage of modified nano-silica sol in the modified nano-silica sol prepared by adopting the formula and preparation method of the specific embodiment is 20% %. The following are the same.
[0039] Its concrete preparation steps of described automobile glass antifogging agent are:
[0040] (1) At room temperature, first add 8 g of glycerin, 5 g of propylene glycol, 15 g of ethanol, 2 g of OP-10 emulsifier, and 1 g of polyethylene glycol into the container. Modified polyacrylate solution 1g, stir well
[0041] (2), then add 0.5g of sodium lauryl sulfate, 0.5g of sodium dodecylbenzenesulfonate, 10g of nano-silica sol, and 57g of water into the container, and then stir evenly to obtain a long-lasting glass anti-fog agent.
[0042] (3), apply this product on th...
Embodiment 2
[0044] A long-acting antifogging agent for automobile glass, which includes the raw materials of the following mass percentages:
[0045]
[0046] The sum of the total mass percentages is 100%. Modified nano-silica sol (20% liquid) means that the mass percentage of modified nano-silica sol in the modified nano-silica sol prepared by adopting the formula and preparation method of the specific embodiment is 20% %.
[0047] The preparation method in this example is identical with example 1.
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